N-Phenyltetrachlorophthalimide

Base Information

• Chemical Name: N-Phenyltetrachlorophthalimide
• CAS No.: 31039-74-4
• Molecular Formula: C14H5 Cl4 N O2
• Molecular Weight: 361.011
• Hs Code.: 2925190090
• Mol file: 31039-74-4.mol

Synonyms:Phthalimide,3,4,5,6-tetrachloro-N-phenyl- (6CI,8CI);3,4,5,6-Tetrachloro-N-phenylphthalimide; 4,5,6,7-Tetrachloro-2-phenylisoindoline-1,3-dione;N-Phenyltetrachlorophthalimide; NSC 263512; Tetrachloro-N-phenylphthalimide

Chemical Property of N-Phenyltetrachlorophthalimide

Chemical Property:

• Vapor Pressure: 2E-11mmHg at 25°C
• Melting Point: 275 °C
• Boiling Point: 532.7 °C at 760 mmHg
• PKA: -4.21±0.20(Predicted)
• Flash Point: 276 °C
• PSA: 37.38000
• Density: 1.682 g/cm³
• LogP: 5.16580

Purity/Quality:

99% ^*data from raw suppliers

N-PHENYLTETRACHLOROPHTHALIMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-Phenyltetrachlorophthalimide

There total 10 articles about N-Phenyltetrachlorophthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.2%

tetrachlorophthalic anhydride (117-08-8) + aniline (62-53-3) → 4,5,6,7-tetrachloro-2-phenylphthalimide (31039-74-4)

Guidance literature:

With cetyltrimethylammonim bromide; In acetic acid; at 120 ℃;

DOI:10.5012/jkcs.2010.54.6.744

Reference yield: 91.0%

N-phenyl benzoyl amide (93-98-1,5705-51-1) → 4,5,6,7-tetrachloro-2-phenylphthalimide (31039-74-4) + benzoic acid (65-85-0,8013-63-6)

Guidance literature:

With tetrachlorophthalic anhydride; at 170 ℃; for 120h;

DOI:10.1016/S0040-4039(00)82395-3

Reference yield: 91.0%

tetrachlorophthalic anhydride (117-08-8) + phenyl isocyanate (103-71-9) → 4,5,6,7-tetrachloro-2-phenylphthalimide (31039-74-4)

Guidance literature:

In N,N-dimethyl acetamide; for 0.0333333h;

upstream raw materials:

tetrachlorophthalic anhydride

aniline

tetrachloro-N-phenylphthalamic acid

N-phenyl benzoyl amide

Downstream raw materials:

4,5,6,7-tetrafluoroisobenzofuran-1,3-dione

tetrafluoro-N-phenylphthalimide

3,4,5,6-tetrafluorophthalic acid

2,3,4,5-tetrafluorobenzoic acid

Refernces

• 1、 Mahapatra, Shankhapani,Singh, Jagadish,Raju, Rajapandi,Maiti, Bhim Charan,Maity, Tapan Kumar. "Evaluation of some synthesized novel substituted phthalimide derivatives as potent antidiabetic agents". experimental part. p. 1581 - 1584. Retrieved 2012/01/13.
• 2、 Li, Hua,Wang, Hongkai,Zhao, Ruiju,Liu, Juan,Zhao, Zhengui,Hu, Guoqin,Liang, Zhengyong. "Preparation of 2,3,4,5-tetrafluorobenzoic acid". experimental part. p. 744 - 748. Retrieved 2011/03/20.