Benzenamine, 5-bromo-2-chloro-3-methoxy-

Base Information

Chemical Name:Benzenamine, 5-bromo-2-chloro-3-methoxy-
CAS No.:63603-12-3
Molecular Formula:C7H7BrClNO
Molecular Weight:236.496
Hs Code.:

Synonyms:

Suppliers and Price of Benzenamine, 5-bromo-2-chloro-3-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of Benzenamine, 5-bromo-2-chloro-3-methoxy-

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenamine, 5-bromo-2-chloro-3-methoxy-

There total 5 articles about Benzenamine, 5-bromo-2-chloro-3-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 63603-12-3
2-chloro-3-methoxy-5-bromoaniline

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / HNO₃, glacial acetic acid / acetic acid / 2 h / Ambient temperature

2: 88 percent / oxalyl chloride / dimethylformamide / -20 deg C; 80 deg C, 3 h

3: 30 g / KOH / ethanol; H₂O / 2 h / 80 °C

4: 60 percent / mercuric oxide, bromine / CCl₄ / 5 h / Irradiation

5: 1.) iron, 2.) HCl / 1.) ethanol, water, 2.) reflux, 12 h

With hydrogenchloride; potassium hydroxide; oxalyl dichloride; bromine; nitric acid; iron; acetic acid; mercury(II) oxide; In tetrachloromethane; ethanol; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ja00353a027

Reference yield:

: 63603-09-8
methyl 4-chloro-3-methoxy-5-nitrobenzoate

: 63603-12-3
2-chloro-3-methoxy-5-bromoaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 30 g / KOH / ethanol; H₂O / 2 h / 80 °C

2: 60 percent / mercuric oxide, bromine / CCl₄ / 5 h / Irradiation

3: 1.) iron, 2.) HCl / 1.) ethanol, water, 2.) reflux, 12 h

With hydrogenchloride; potassium hydroxide; bromine; iron; mercury(II) oxide; In tetrachloromethane; ethanol; water;
DOI:10.1021/ja00353a027

Reference yield:

: 42590-00-1
4-hydroxy-3-methoxy-5-nitrobenzoic acid methyl ester

: 63603-12-3
2-chloro-3-methoxy-5-bromoaniline

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / oxalyl chloride / dimethylformamide / -20 deg C; 80 deg C, 3 h

2: 30 g / KOH / ethanol; H₂O / 2 h / 80 °C

3: 60 percent / mercuric oxide, bromine / CCl₄ / 5 h / Irradiation

4: 1.) iron, 2.) HCl / 1.) ethanol, water, 2.) reflux, 12 h

With hydrogenchloride; potassium hydroxide; oxalyl dichloride; bromine; iron; mercury(II) oxide; In tetrachloromethane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00353a027