L-Phenylalanine, N-(methylsulfonyl)-, 4-cyclopentene-1,3-diyl ester, cis-

Base Information

Chemical Name:L-Phenylalanine, N-(methylsulfonyl)-, 4-cyclopentene-1,3-diyl ester, cis-
CAS No.:63603-17-8
Molecular Formula:C25H30N2O8S2
Molecular Weight:550.654
Hs Code.:

Synonyms:

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Chemical Property of L-Phenylalanine, N-(methylsulfonyl)-, 4-cyclopentene-1,3-diyl ester, cis-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of L-Phenylalanine, N-(methylsulfonyl)-, 4-cyclopentene-1,3-diyl ester, cis-

There total 5 articles about L-Phenylalanine, N-(methylsulfonyl)-, 4-cyclopentene-1,3-diyl ester, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 29783-26-4
cis-4-cyclopentene-1,3-diol

: 63640-54-0
(+)-N-mesyl-(S)-phenylalanyl chloride

: 63603-18-9,63640-55-1
(+)-4(S)-hydroxy-2-cyclopenten-1(R)-yl N-mesyl-(S)-phenylalaninate

: 63603-17-8
(-)-2-cyclopenten-1(R),4(S)-diyl bis-N-mesyl-(S)-phenylalaninate

: 63603-18-9,63640-55-1
(-)-4(R)-hydroxy-2-cyclopenten-1(S)-yl N-mesyl-(S)-phenylalaninate

Guidance literature:: With pyridine; Ambient temperature;
DOI:10.1016/0040-4020(80)80160-8

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 63603-17-8
(-)-2-cyclopenten-1(R),4(S)-diyl bis-N-mesyl-(S)-phenylalaninate

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NaOH / H₂O / 1.5 h

2: 87 percent / PCl₅ / benzene / in ice bath, 2 h then at r.t., 1 h

3: 24 percent / pyridine / Ambient temperature

With pyridine; sodium hydroxide; phosphorus pentachloride; In water; benzene;
DOI:10.1016/0040-4020(80)80160-8

Reference yield:

: 42361-65-9
N-(methylsulfonyl)-L-phenylalanine

: 63603-17-8
(-)-2-cyclopenten-1(R),4(S)-diyl bis-N-mesyl-(S)-phenylalaninate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / PCl₅ / benzene / in ice bath, 2 h then at r.t., 1 h

2: 24 percent / pyridine / Ambient temperature

With pyridine; phosphorus pentachloride; In benzene;
DOI:10.1016/0040-4020(80)80160-8