Benzeneacetic acid, 3,4-dimethylphenyl ester

Base Information

• Chemical Name: Benzeneacetic acid, 3,4-dimethylphenyl ester
• CAS No.: 63609-36-9
• Molecular Formula: C₁₆H₁₆O₂
• Molecular Weight: 240.302
• Mol file: 63609-36-9.mol

Synonyms:

Chemical Property of Benzeneacetic acid, 3,4-dimethylphenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzeneacetic acid, 3,4-dimethylphenyl ester

There total 1 articles about Benzeneacetic acid, 3,4-dimethylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-Dimethylphenol (95-65-8) + phenylacetyl chloride (103-80-0) → 3,4-Dimethylphenylacetat (63609-36-9)

Guidance literature:

With pyridine;

DOI:10.1021/jo00443a043

Reference yield:

3,4-Dimethylphenylacetat (63609-36-9) → 2-Methoxy-4,5-Dimethylstilben (63609-32-5)

Guidance literature:

Multi-step reaction with 4 steps

1: AlCl₃

2: aq. KOH

3: LiAlH₄

4: dimethylsulfoxide / 140 °C

With potassium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; In dimethyl sulfoxide;

DOI:10.1021/jo00443a043

Reference yield:

3,4-Dimethylphenylacetat (63609-36-9) → 2,3-dimethylphenanthrene (3674-65-5)

Guidance literature:

Multi-step reaction with 5 steps

1: AlCl₃

2: aq. KOH

3: LiAlH₄

4: dimethylsulfoxide / 140 °C

5: I₂ / cyclohexane / Irradiation

With potassium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; iodine; In cyclohexane; dimethyl sulfoxide;

DOI:10.1021/jo00443a043

upstream raw materials:

3,4-Dimethylphenol

phenylacetyl chloride

Downstream raw materials:

2-phenylacetyl-4,5-dimethylphenol

2,3-dimethylphenanthrene

2-methoxy-4,5-dimethyl-deoxybenzoin

1-(2-Methoxy-4,5-dimethyl-phenyl)-2-phenyl-ethanol