1-Naphthylamine, 1,2,3,4-tetrahydro-, hydrochloride

Base Information

• Chemical Name: 1-Naphthylamine, 1,2,3,4-tetrahydro-, hydrochloride
• CAS No.: 3459-02-7
• Molecular Formula: C10H13N
• Molecular Weight: 183.681
• Mol file: 3459-02-7.mol

Synonyms:1-NAPHTHYLAMINE, 1,2,3,4-TETRAHYDRO-, HYDROCHLORIDE;EINECS 222-397-1;1,2,3,4-tetrahydronaphthalen-1-ylazanium;chloride;LS-95831

Chemical Property of 1-Naphthylamine, 1,2,3,4-tetrahydro-, hydrochloride

Chemical Property:

• Vapor Pressure: 0.0228mmHg at 25°C
• Melting Point: 181-187℃
• Boiling Point: 249.6°Cat760mmHg
• Flash Point: 110.8°C
• PSA: 26.02000
• Density: 1.023g/cm³
• LogP: 3.52500
• Storage Temp.: Inert atmosphere,Room Temperature
• Sensitive.: Hygroscopic
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 183.0814771
• Heavy Atom Count: 12
• Complexity: 133

Purity/Quality:

99%, ^*data from raw suppliers

1,2,3,4-Tetrahydro-1-naphthylaminehydrochloride98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC(C2=CC=CC=C2C1)[NH3+].[Cl-]

Technology Process of 1-Naphthylamine, 1,2,3,4-tetrahydro-, hydrochloride

There total 2 articles about 1-Naphthylamine, 1,2,3,4-tetrahydro-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

tetralin (119-64-2) → 1,2,3,4-tetrahydro-1-naphthylamine hydrochloride (3459-02-7,49800-23-9,32908-42-2)

Guidance literature:

tetralin; With Benzophenone imine; copper(l) iodide; 1,10-Phenanthroline; di-tert-butyl peroxide; In chlorobenzene; at 90 ℃; for 48h; Inert atmosphere; Sealed tube;

With hydrogenchloride; In methanol; water; chlorobenzene; at 40 ℃; for 15h; regioselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.orglett.8b03505

Reference yield:

→ 1,2,3,4-tetrahydro-1-naphthylamine hydrochloride (3459-02-7,49800-23-9,32908-42-2)

Guidance literature:

1.2.3.4-Tetrahydronaphthalin-1-on, (-> Oxim), Red. mit H2, Pd/C;

DOI:10.1021/jm00267a010

Reference yield: 56.0%

1,2,3,4-tetrahydro-1-naphthylamine hydrochloride (3459-02-7,49800-23-9,32908-42-2) + 4-benzyl-1-(3-chloropropyl)piperidine (136718-81-5) → N-[3-(4-benzyl-1-piperidinyl)propyl]-1,2,3,4-tetrahydro-1-naphthylamine dihydrochloride

Guidance literature:

With triethylamine;

upstream raw materials:

tetralin

Downstream raw materials:

1,2,3,4-tetrahydronaphthalen-1-amine

(S)-1,2,3,4-tetrahydro-1-naphthylamine hydrogen D-tartrate

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