N,N-Dichloro-1-phenylmethanesulfonamide

Base Information

• Chemical Name: N,N-Dichloro-1-phenylmethanesulfonamide
• CAS No.: 63636-97-5
• Molecular Formula: C7H7Cl2NO2S
• Molecular Weight: 240.11
• DSSTox Substance ID: DTXSID20502970
• Wikidata: Q82356417
• Mol file: 63636-97-5.mol

Synonyms:N,N-Dichloro-1-phenylmethanesulfonamide;63636-97-5;SCHEMBL8840586;DTXSID20502970;N,N-dichlorophenylmethanesulfonamide

Chemical Property of N,N-Dichloro-1-phenylmethanesulfonamide

Chemical Property:

• XLogP3: 2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 238.9574550
• Heavy Atom Count: 13
• Complexity: 242

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CS(=O)(=O)N(Cl)Cl

Technology Process of N,N-Dichloro-1-phenylmethanesulfonamide

There total 1 articles about N,N-Dichloro-1-phenylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

phenyl-methanesulfonic acid amide (4563-33-1) → N,N-dichlorophenylmethanesulfonamide (63636-97-5)

Guidance literature:

With chlorine; sodium hydroxide; In water; at 20 ℃; for 2h;

DOI:10.1134/S107042801204001X

Reference yield: 95.0%

Trichloroethylene (79-01-6) + N,N-dichlorophenylmethanesulfonamide (63636-97-5) → phenyl-N-(2,2,2-trichloroethylidene)methanesulfonamide (90348-89-3)

Guidance literature:

at 90 - 92 ℃; Inert atmosphere;

DOI:10.1134/S107042801204001X

Reference yield:

N,N-dichlorophenylmethanesulfonamide (63636-97-5) → Methoxychlor (72-43-5,105367-23-5) + phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide (1376938-31-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 - 92 °C / Inert atmosphere

2: phosphorus pentoxide; sulfuric acid

With phosphorus pentoxide; sulfuric acid;

DOI:10.1134/S107042801204001X

upstream raw materials:

phenyl-methanesulfonic acid amide

Downstream raw materials:

phenyl-N-[2,2,2-trichloro-1-(4-methylphenyl)ethyl]methanesulfonamide

Methylchlor

phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide

Methoxychlor