phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide

Base Information

Chemical Name:phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide
CAS No.:1376938-31-6
Molecular Formula:C₁₆H₁₆Cl₃NO₃S
Molecular Weight:408.733
Hs Code.:

Synonyms:phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide

Chemical Property:

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Technology Process of phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide

There total 6 articles about phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 90348-89-3
phenyl-N-(2,2,2-trichloroethylidene)methanesulfonamide

: 100-66-3
methoxybenzene

: 1376938-31-6
phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide

Guidance literature:: With phosphorus pentoxide; sulfuric acid; In tetrachloromethane; for 3h;
DOI:10.1134/S107042801204001X

Reference yield:

: 4563-33-1
phenyl-methanesulfonic acid amide

: 72-43-5,105367-23-5
Methoxychlor

: 1376938-31-6
phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: chlorine; sodium hydroxide / water / 2 h / 20 °C

2: 90 - 92 °C / Inert atmosphere

3: phosphorus pentoxide; sulfuric acid

With phosphorus pentoxide; sulfuric acid; chlorine; sodium hydroxide; In water;
DOI:10.1134/S107042801204001X

Reference yield:

: 63636-97-5
N,N-dichlorophenylmethanesulfonamide

: 72-43-5,105367-23-5
Methoxychlor

: 1376938-31-6
phenyl-N-[2,2,2-trichloro-1-(4-methoxyphenyl)ethyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 - 92 °C / Inert atmosphere

2: phosphorus pentoxide; sulfuric acid

With phosphorus pentoxide; sulfuric acid;
DOI:10.1134/S107042801204001X