Technology Process of 1-[(Triphenylstannyl)methyl]cyclohexan-1-ol
There total 1 articles about 1-[(Triphenylstannyl)methyl]cyclohexan-1-ol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
diethyl ether; hexane;
under N2 n-BuLi/hexane added at -50°C for 1 min, stirred for 8 min, cyclohexanone/ether added at -50°C, stirred for 10 min, allowed to room temp., hydrolysis with H2O; extd. (CHCl3), dried on Na2SO4, concd. in vac., dissolved in petroether, cooled to -30°C for crystn., recrystd. (petroether), elem. anal.;