5H-Dibenzo(a,d)cycloheptene-4-methylamine 10,11-dihydro-N,N-dimethyl-5-methylene-

Base Information

Chemical Name:5H-Dibenzo(a,d)cycloheptene-4-methylamine 10,11-dihydro-N,N-dimethyl-5-methylene-
CAS No.:33953-64-9
Molecular Formula:C19H21N
Molecular Weight:0
Hs Code.:
DSSTox Substance ID:DTXSID90187571
Nikkaji Number:J42.171E
Wikidata:Q83059275
Mol file:33953-64-9.mol

Synonyms:BRN 2944467;5H-Dibenzo(a,d)cycloheptene-4-methylamine 10,11-dihydro-N,N-dimethyl-5-methylene-;33953-64-9;10,11-Dihydro-N,N-dimethyl-5-methylene-5H-dibenzo(a,d)cycloheptene-4-methylamine;DTXSID90187571;LS-60725;10,11-Dihydro-N,N-dimethyl-5-methylene-5H-dibenzo[a,d]cycloheptene-4-methanamine;5H-Dibenzo[a,d]cycloheptene-4-methanamine, 10,11-dihydro-N,N-dimethyl-5-methylene-

Suppliers and Price of 5H-Dibenzo(a,d)cycloheptene-4-methylamine 10,11-dihydro-N,N-dimethyl-5-methylene-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5H-Dibenzo(a,d)cycloheptene-4-methylamine 10,11-dihydro-N,N-dimethyl-5-methylene-

Chemical Property:

Vapor Pressure:8.92E-06mmHg at 25°C
Boiling Point:373.5°C at 760 mmHg
Flash Point:161.6°C
PSA：3.24000
Density:1.06g/cm³
LogP:3.90830
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:263.167399674
Heavy Atom Count:20
Complexity:346

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C)CC1=CC=CC2=C1C(=C)C3=CC=CC=C3CC2

Technology Process of 5H-Dibenzo(a,d)cycloheptene-4-methylamine 10,11-dihydro-N,N-dimethyl-5-methylene-

There total 2 articles about 5H-Dibenzo(a,d)cycloheptene-4-methylamine 10,11-dihydro-N,N-dimethyl-5-methylene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,2-Dimethyl-1,2,3,7,8,12b-hexahydrobenzo<6,7>cyclohepta<1,2,3-d,e>isochinolinium

: 33953-64-9
10,11-Dihydro-N,N-dimethyl-5-methylen-5H-dibenzocyclohepten-4-methylamin

Guidance literature:: With ion-exchange resin - form>; In methanol; water;
DOI:10.1021/jm00292a024

Reference yield:

: 33953-64-9
10,11-Dihydro-N,N-dimethyl-5-methylen-5H-dibenzocyclohepten-4-methylamin

Guidance literature:: quart. Salz III, bas. Ionenaustauscher;

Reference yield:

: 33953-64-9
10,11-Dihydro-N,N-dimethyl-5-methylen-5H-dibenzocyclohepten-4-methylamin

: 36189-16-9
Methyl-[3-(5-methylene-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-4-yl)-propyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: ClCO₂Et / benzene

2: (i) NaOEt, EtOH, (ii) /BRN= 1969585/

3: (i) aq. KOH, EtOH, (ii) (heating)

4: (i) SOCl₂, DMF, (ii) /BRN= 3589311/, aq. NaOH, benzene

5: LiAlH₄ / tetrahydrofuran

6: benzene

With lithium aluminium tetrahydride; chloroformic acid ethyl ester; In tetrahydrofuran; benzene;
DOI:10.1021/jm00292a024