(2-Amino-5-methylphenyl)phosphonic acid

Base Information

Chemical Name:(2-Amino-5-methylphenyl)phosphonic acid
CAS No.:69675-98-5
Molecular Formula:C7H10NO3P
Molecular Weight:187.135
Hs Code.:
European Community (EC) Number:839-661-2
NSC Number:87208
DSSTox Substance ID:DTXSID80293099
Nikkaji Number:J3.164.186A
Wikidata:Q82031698

Synonyms:(2-amino-5-methylphenyl)phosphonic acid;69675-98-5;NSC87208;(2-amino-5-methyl-phenyl)phosphonic acid;C7H10NO3P;SCHEMBL17607326;DTXSID80293099;MFCD20699745;NSC-87208;AKOS028111199;(2-amino-5-methylphenyl)phosphonicacid;CS-0058758;D83786;EN300-252339

Suppliers and Price of (2-Amino-5-methylphenyl)phosphonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of (2-Amino-5-methylphenyl)phosphonic acid

Chemical Property:

Vapor Pressure:1.62E-08mmHg at 25°C
Boiling Point:440°Cat760mmHg
Flash Point:219.9°C
Density:1.43g/cm³
XLogP3:0.2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:187.03983018
Heavy Atom Count:12
Complexity:203

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)N)P(=O)(O)O

Technology Process of (2-Amino-5-methylphenyl)phosphonic acid

There total 3 articles about (2-Amino-5-methylphenyl)phosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 42822-58-2
2-amino-5-methyl-phenylphosphonic acid diethylester

: 69675-98-5
(2-amino-5-methylphenyl)phosphonic acid

Guidance literature:: With trimethylsilyl bromide; In acetonitrile; at 25 ℃; for 16h; Inert atmosphere;

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 69675-98-5
(2-amino-5-methylphenyl)phosphonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate; iodine / water; dichloromethane / 22 h / 0 - 25 °C / Inert atmosphere

2: potassium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide / toluene / 18 h / 110 °C / Inert atmosphere

3: trimethylsilyl bromide / acetonitrile / 16 h / 25 °C / Inert atmosphere

With copper(l) iodide; trimethylsilyl bromide; iodine; sodium hydrogencarbonate; potassium carbonate; N,N`-dimethylethylenediamine; In dichloromethane; water; toluene; acetonitrile;