2-amino-5-methyl-phenylphosphonic acid diethylester

Base Information

Chemical Name:2-amino-5-methyl-phenylphosphonic acid diethylester
CAS No.:42822-58-2
Molecular Formula:C₁₁H₁₈NO₃P
Molecular Weight:243.243
Hs Code.:

Synonyms:2-amino-5-methyl-phenylphosphonic acid diethylester

Suppliers and Price of 2-amino-5-methyl-phenylphosphonic acid diethylester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-amino-5-methyl-phenylphosphonic acid diethylester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-amino-5-methyl-phenylphosphonic acid diethylester

There total 8 articles about 2-amino-5-methyl-phenylphosphonic acid diethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Diethyl phosphonate: 762-04-9,123-22-8
Diethyl phosphonate

: 29289-13-2
2-iodo-4-methylaniline

: 42822-58-2
2-amino-5-methyl-phenylphosphonic acid diethylester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In toluene; at 100 ℃; for 14h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tetlet.2012.07.037

Reference yield: 76.0%

Diethyl phosphonate: 762-04-9,123-22-8
Diethyl phosphonate

2-bromo-p-toluidine: 583-68-6
2-bromo-p-toluidine

: 42822-58-2
2-amino-5-methyl-phenylphosphonic acid diethylester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In toluene; at 100 ℃; for 14h;
DOI:10.1016/j.jorganchem.2014.04.014

Reference yield: 72.0%

: 29289-13-2
2-iodo-4-methylaniline

: 762-04-9
phosphonic acid diethyl ester

: 42822-58-2
2-amino-5-methyl-phenylphosphonic acid diethylester

Guidance literature:: With copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine; In toluene; at 110 ℃; for 14h; Inert atmosphere; Large scale;
DOI:10.1002/ejic.201300342