Bis(4-propylphenyl)methanone

Base Information

• Chemical Name: Bis(4-propylphenyl)methanone
• CAS No.: 64357-93-3
• Molecular Formula: C19H22O
• Molecular Weight: 266.383
• DSSTox Substance ID: DTXSID80556631
• Wikidata: Q82438251
• Mol file: 64357-93-3.mol

Synonyms:Bis(4-propylphenyl)methanone;64357-93-3;SCHEMBL9861628;DTXSID80556631

Chemical Property of Bis(4-propylphenyl)methanone

Chemical Property:

• XLogP3: 5.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 266.167065321
• Heavy Atom Count: 20
• Complexity: 252

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC1=CC=C(C=C1)C(=O)C2=CC=C(C=C2)CCC

Technology Process of Bis(4-propylphenyl)methanone

There total 5 articles about Bis(4-propylphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4.4'-Dipropyl-benzhydrol (108396-05-0) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → hexahydro-2H-oxepin-2-one (502-44-3,24980-41-4,80137-66-2) + 4,4'-di-n-propylbenzophenone (64357-93-3)

Guidance literature:

4.4'-Dipropyl-benzhydrol; cyclohexanone; With N-hydroxyphthalimide; 2,2'-azobis(isobutyronitrile); oxygen; In ethyl acetate; at 75 ℃; for 8h;

With bis(3-trifluoromethyl) diselenide; In 2,2,2-trifluoroethanol; ethyl acetate; at 30 ℃; for 6h;

Reference yield: 41.0%

carbon monoxide (201230-82-2) + 4-propylphenylboric acid (134150-01-9) → 4,4'-di-n-propylbenzophenone (64357-93-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-bis-(diphenylphosphino)propane; silver nitrate; In acetone; at 40 ℃; for 36h; under 760.051 Torr; Autoclave; Inert atmosphere;

DOI:10.1055/s-0033-1340957

Reference yield:

phenylpropane (103-65-1) + 4-propylbenzoyl chloride (52710-27-7) → 4,4'-di-n-propylbenzophenone (64357-93-3)

Guidance literature:

With aluminium trichloride;

DOI:10.1039/jr9520003741

upstream raw materials:

phenylpropane

4-propylbenzoyl chloride

carbon monoxide

4-propylphenylboric acid

Downstream raw materials:

<2-Dimethylamino-aethyl>-<4.4'-dipropyl-benzhydryl>-aether

4.4'-Dipropyl-benzhydrol

C₃₄H₃₄