N-BUTYLSUCCINIMIDE

Base Information

• Chemical Name: N-BUTYLSUCCINIMIDE
• CAS No.: 3470-96-0
• Molecular Formula: C8H13 N O2
• Molecular Weight: 155.197
• Hs Code.: 2925190090
• Mol file: 3470-96-0.mol

Synonyms:Succinimide,N-butyl- (6CI,7CI,8CI); N-Butylsuccinimide; NSC 38157

Chemical Property of N-BUTYLSUCCINIMIDE

Chemical Property:

• Vapor Pressure: 0.00712mmHg at 25°C
• Boiling Point: 269.8°Cat760mmHg
• Flash Point: 116.8°C
• PSA: 37.38000
• Density: 1.082g/cm³
• LogP: 0.87340

Purity/Quality:

N-BUTYLSUCCINIMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-BUTYLSUCCINIMIDE

There total 2 articles about N-BUTYLSUCCINIMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

1-bromo-butane (109-65-9) + N-Bromosuccinimide (128-08-5) → Succinimide (123-56-8,89963-74-6) + N-butylsuccinimide (3470-96-0)

Guidance literature:

With tetrabutylammonium tetrafluoroborate; In acetonitrile; for 3h; Product distribution; reduction by -0.8 V; other alkylating reagents and reagents;

DOI:10.1021/jo00346a026

Reference yield:

tetra-N-butylammonium salt of succinimide (74830-30-1) → N-butylsuccinimide (3470-96-0) + tributyl-amine (102-82-9)

Guidance literature:

With tetrafluoroboric acid; In N,N-dimethyl-formamide; for 20h; Yield given; Heating;

DOI:10.1016/S0040-4020(01)93685-3

Reference yield:

N-butylsuccinimide (3470-96-0) → 1-butylpyrrolidine (767-10-2)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

DOI:10.1021/jo01371a002

upstream raw materials:

1-bromo-butane

N-Bromosuccinimide

tetra-N-butylammonium salt of succinimide

Downstream raw materials:

1-butylpyrrolidine

N-butylsuccinamide

1-Butyl-5-hydroxy-5-(3-trifluoromethyl-phenyl)-pyrrolidin-2-one

5-(3-benzyloxy-propyl)-1-butyl-5-methoxy-pyrrolidin-2-one