1-[(E)-2-(benzenesulfonyl)ethenyl]-4-phenylbenzene

Base Information

Chemical Name:1-[(E)-2-(benzenesulfonyl)ethenyl]-4-phenylbenzene
CAS No.:30166-77-9
Molecular Formula:C20H16 O2 S
Molecular Weight:320.4048
Hs Code.:
NSC Number:140154
DSSTox Substance ID:DTXSID30419247
Wikidata:Q82230193
Mol file:30166-77-9.mol

Synonyms:NSC140154;30166-77-9;DTXSID30419247;NSC-140154

Suppliers and Price of 1-[(E)-2-(benzenesulfonyl)ethenyl]-4-phenylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-[(E)-2-(benzenesulfonyl)ethenyl]-4-phenylbenzene

Chemical Property:

Vapor Pressure:2.92E-11mmHg at 25°C
Boiling Point:542°C at 760 mmHg
Flash Point:347.5°C
Density:1.207g/cm³
XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:320.08710092
Heavy Atom Count:23
Complexity:468

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC=C(C=C2)C=CS(=O)(=O)C3=CC=CC=C3
Isomeric SMILES:C1=CC=C(C=C1)C2=CC=C(C=C2)/C=C/S(=O)(=O)C3=CC=CC=C3

Technology Process of 1-[(E)-2-(benzenesulfonyl)ethenyl]-4-phenylbenzene

There total 4 articles about 1-[(E)-2-(benzenesulfonyl)ethenyl]-4-phenylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 32340-38-8
biphenyl-4-yl-propynoic acid

: 98-80-6
phenylboronic acid

: 30166-77-9
(E)‐4‐(2-(phenylsulfonyl)vinyl)-1,1'-biphenyl

Guidance literature:: With 1,10-Phenanthroline; potassium pyrosulfite; acetic acid; copper(ll) bromide; In 1,2-dimethoxyethane; at 100 ℃; for 17h;
DOI:10.1039/d1ob01435h

Reference yield: 31.0%

: 3112-85-4
methylphenylsulfonate

: 3218-36-8
4-Phenylbenzaldehyde

: 30166-77-9
(E)‐4‐(2-(phenylsulfonyl)vinyl)-1,1'-biphenyl

Guidance literature:: methylphenylsulfonate; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.166667h;

With diethyl chlorophosphate; In tetrahydrofuran; hexane; at 0 ℃; for 0.166667h;

4-Phenylbenzaldehyde; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 16h;
DOI:10.1021/acs.orglett.1c01794