Benzenepropanoic acid, b-(2-amino-2-oxoethyl)-

Base Information

Chemical Name:Benzenepropanoic acid, b-(2-amino-2-oxoethyl)-
CAS No.:6456-86-6
Molecular Formula:C11H13NO3
Molecular Weight:207.229
Hs Code.:

Synonyms:5-amino-5-oxo-3-phenylpentanoic acid;3-phenyl-glutaramic acid;β-Phenyl-glutarsaeuremonoamid;3-Phenyl-glutaramidsaeure;

Suppliers and Price of Benzenepropanoic acid, b-(2-amino-2-oxoethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Benzenepropanoic acid, b-(2-amino-2-oxoethyl)-

Chemical Property:

PSA：80.39000
LogP:1.82060

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenepropanoic acid, b-(2-amino-2-oxoethyl)-

There total 8 articles about Benzenepropanoic acid, b-(2-amino-2-oxoethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 4160-80-9
3-phenylglutaric acid anhydride

: 6456-86-6
4-(aminocarbonyl)-3-phenylbutanoic acid

Guidance literature:: With ammonia; In benzene; Ambient temperature;

Reference yield:

: 78533-83-2
3-Phenylpentandiamid

: 6456-86-6
4-(aminocarbonyl)-3-phenylbutanoic acid

Guidance literature:: With hydrogenchloride; In water; at 95 ℃;
DOI:10.1002/adsc.201800956

Reference yield:

: 100-52-7
benzaldehyde

: 6456-86-6
4-(aminocarbonyl)-3-phenylbutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: piperidine / 72 h / 20 °C

2: potassium hydroxide / water / 2 h / 80 °C

3: acetyl chloride / 2 h / Reflux

4: ammonium hydroxide / tetrahydrofuran / 20 °C

With piperidine; ammonium hydroxide; acetyl chloride; potassium hydroxide; In tetrahydrofuran; water;
DOI:10.1039/c4md00498a