Cycliton

Base Information

• Chemical Name: Cycliton
• CAS No.: 2433-20-7
• Molecular Formula: C₁₀H₁₆N₂O₂
• Molecular Weight: 196.249
• Hs Code.: 2934999090
• DSSTox Substance ID: DTXSID80179066
• Nikkaji Number: J21.587B
• Wikidata: Q83049594
• Mol file: 2433-20-7.mol

Synonyms:CYCLITON;Oxalept;2433-20-7;N,N-diethyl-3,5-dimethyl-1,2-oxazole-4-carboxamide;DTXSID80179066;AKOS006243263;4-Isoxazolecarboxamide, N,N-diethyl-3,5-dimethyl-

Chemical Property of Cycliton

Chemical Property:

• Vapor Pressure: 3.7E-05mmHg at 25°C
• Boiling Point: 353°Cat760mmHg
• Flash Point: 167.3°C
• PSA: 46.34000
• Density: 1.053g/cm³
• LogP: 1.77340
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 196.121177757
• Heavy Atom Count: 14
• Complexity: 204

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)C(=O)C1=C(ON=C1C)C

Technology Process of Cycliton

There total 3 articles about Cycliton which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethylisoxazole-4-carbonyl chloride (31301-45-8) + diethylamine (109-89-7) → 3,5-dimethyl-isoxazole-4-carboxylic acid diethylamide (2433-20-7)

Guidance literature:

With diethyl ether;

Reference yield:

3,5-dimethyl-4-isoxazolecarboxylic acid (2510-36-3) → 3,5-dimethyl-isoxazole-4-carboxylic acid diethylamide (2433-20-7)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂

2: diethyl ether

With thionyl chloride; diethyl ether;

Reference yield:

3,3'-ethanediyldiamino-di-crotonic acid bis-diethylamide + acetic anhydride (108-24-7) → 3,5-dimethyl-isoxazole-4-carboxylic acid diethylamide (2433-20-7)

Guidance literature:

Erwaermen des Reaktionsgemisches mit (NH₂OH)2+H₂SO₄ in wss. Methanol;

upstream raw materials:

3,5-dimethylisoxazole-4-carbonyl chloride

diethylamine

acetic anhydride

3,5-dimethyl-4-isoxazolecarboxylic acid