(E)-N-(2,4-Dimethylpent-3-en-2-yl)-1-phenylmethanimine

Base Information

Chemical Name:(E)-N-(2,4-Dimethylpent-3-en-2-yl)-1-phenylmethanimine
CAS No.:64760-60-7
Molecular Formula:C14H19N
Molecular Weight:201.312
Hs Code.:
DSSTox Substance ID:DTXSID20507546

Synonyms:64760-60-7;(E)-N-(2,4-Dimethylpent-3-en-2-yl)-1-phenylmethanimine;DTXSID20507546

Suppliers and Price of (E)-N-(2,4-Dimethylpent-3-en-2-yl)-1-phenylmethanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of (E)-N-(2,4-Dimethylpent-3-en-2-yl)-1-phenylmethanimine

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:201.151749610
Heavy Atom Count:15
Complexity:238

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC(C)(C)N=CC1=CC=CC=C1)C

Technology Process of (E)-N-(2,4-Dimethylpent-3-en-2-yl)-1-phenylmethanimine

There total 5 articles about (E)-N-(2,4-Dimethylpent-3-en-2-yl)-1-phenylmethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 100-52-7
benzaldehyde

: 64760-62-9
2-amino-2,4-dimethyl-3-pentene

: 64760-60-7
2-aza-3,3,5-trimethyl-1-phenyl-1,4-hexadiene

Guidance literature:: at 100 ℃; for 10h;
DOI:10.1021/ja00401a037

Reference yield:

: 924-50-5
Methyl 3,3-dimethylacrylate

: 64760-60-7
2-aza-3,3,5-trimethyl-1-phenyl-1,4-hexadiene

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / diethyl ether / 1 h / 0 °C

2: 74 percent / NaN₃, conc. H₂SO₄ / CHCl₃ / 0.17 h

3: 50 percent / LiAlH₄ / diethyl ether / 1 h / 0 °C

4: 54 percent / 10 h / 100 °C

With lithium aluminium tetrahydride; sodium azide; sulfuric acid; In diethyl ether; chloroform;
DOI:10.1021/ja00401a037

Reference yield:

: 56763-70-3
2,4-dimethyl-3-penten-2-ol

: 64760-60-7
2-aza-3,3,5-trimethyl-1-phenyl-1,4-hexadiene

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / NaN₃, conc. H₂SO₄ / CHCl₃ / 0.17 h

2: 50 percent / LiAlH₄ / diethyl ether / 1 h / 0 °C

3: 54 percent / 10 h / 100 °C

With lithium aluminium tetrahydride; sodium azide; sulfuric acid; In diethyl ether; chloroform;
DOI:10.1021/ja00401a037