2-methyl-4-oxo-1,4-dihydropyridin-3-yl acetate

Base Information

Chemical Name:2-methyl-4-oxo-1,4-dihydropyridin-3-yl acetate
CAS No.:17184-20-2
Molecular Formula:C₈H₉NO₃
Molecular Weight:167.164
Hs Code.:
Mol file:17184-20-2.mol

Synonyms:4(1H)-Pyridone,3-hydroxy-2-methyl-, acetate (7CI); 4(1H)-Pyridone, 3-hydroxy-2-methyl-,acetate (ester) (8CI); NSC 291920

Suppliers and Price of 2-methyl-4-oxo-1,4-dihydropyridin-3-yl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-methyl-4-oxo-1,4-dihydropyridin-3-yl acetate

Chemical Property:

Vapor Pressure:0.00336mmHg at 25°C
Boiling Point:282.4°Cat760mmHg
Flash Point:124.6°C
Density:1.21g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-methyl-4-oxo-1,4-dihydropyridin-3-yl acetate

There total 5 articles about 2-methyl-4-oxo-1,4-dihydropyridin-3-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 17184-19-9
3-hydroxy-2-methylpyrid-4-one

: 108-24-7
acetic anhydride

: 17184-20-2
2-methyl-3-acetoxy-4(1H)-pyridone

Guidance literature:: at 130 - 140 ℃; for 21h;
DOI:10.1002/jps.2600690923

Reference yield:

: 118-71-8
Maltol

: 17184-20-2
2-methyl-3-acetoxy-4(1H)-pyridone

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent

2: 80.5 percent / NH₄OH / 1.) refluxm 12 h, 2.) room temperature, 4 h

3: 77 percent / 48percent HBr / 4 h / 140 - 150 °C

4: 22 percent / 21 h / 130 - 140 °C

With ammonium hydroxide; hydrogen bromide;
DOI:10.1002/jps.2600690923

Reference yield:

: 4780-14-7
3-methoxy-2-methyl-4-pyrone

: 17184-20-2
2-methyl-3-acetoxy-4(1H)-pyridone

Guidance literature:: Multi-step reaction with 3 steps

1: 80.5 percent / NH₄OH / 1.) refluxm 12 h, 2.) room temperature, 4 h

2: 77 percent / 48percent HBr / 4 h / 140 - 150 °C

3: 22 percent / 21 h / 130 - 140 °C

With ammonium hydroxide; hydrogen bromide;
DOI:10.1002/jps.2600690923