L-Tyrosine, N-[3-(3,4-dimethoxyphenyl)-1-oxo-2-propenyl]-3-methoxy-O-methyl-, methyl ester, (E)-

Base Information

Chemical Name:L-Tyrosine, N-[3-(3,4-dimethoxyphenyl)-1-oxo-2-propenyl]-3-methoxy-O-methyl-, methyl ester, (E)-
CAS No.:64803-83-4
Molecular Formula:C23H27NO7
Molecular Weight:429.47
Hs Code.:

Synonyms:

Suppliers and Price of L-Tyrosine, N-[3-(3,4-dimethoxyphenyl)-1-oxo-2-propenyl]-3-methoxy-O-methyl-, methyl ester, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of L-Tyrosine, N-[3-(3,4-dimethoxyphenyl)-1-oxo-2-propenyl]-3-methoxy-O-methyl-, methyl ester, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of L-Tyrosine, N-[3-(3,4-dimethoxyphenyl)-1-oxo-2-propenyl]-3-methoxy-O-methyl-, methyl ester, (E)-

There total 5 articles about L-Tyrosine, N-[3-(3,4-dimethoxyphenyl)-1-oxo-2-propenyl]-3-methoxy-O-methyl-, methyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53755-02-5
3-(3,4-dihydroxy-phenyl)-2-[3-(3,4-dihydroxy-phenyl)-acryloylamino]propionic acid

: 74-88-4
methyl iodide

: 64803-83-4
pentamethyl-trans-clovamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2018.04.044

Reference yield:

: 1421-65-4
L-dopa methyl ester hydrochloride

: 64803-83-4
pentamethyl-trans-clovamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane; N,N-dimethyl-formamide / 0.25 h / Inert atmosphere; Cooling with ice

1.2: 19 h / 20 °C / Inert atmosphere

2.1: lithium hydroxide / tetrahydrofuran; water / 9 h / 45 °C / Inert atmosphere

2.2: Dowex / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2018.04.044

Reference yield:

: 120094-83-9
(S)-3-(3,4-dihydroxyphenyl)-2-[3-(3,4-dihydroxyphenyl)acryloylamino]propionic acid methyl ester

: 64803-83-4
pentamethyl-trans-clovamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hydroxide / tetrahydrofuran; water / 9 h / 45 °C / Inert atmosphere

1.2: Dowex / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With potassium carbonate; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2018.04.044