3,4-Dimethyl-2-nitroaniline

Base Information

Chemical Name:3,4-Dimethyl-2-nitroaniline
CAS No.:64823-23-0
Molecular Formula:C8H10N2O2
Molecular Weight:166.18
Hs Code.:2921430090
DSSTox Substance ID:DTXSID001303758
Nikkaji Number:J141.324D
Mol file:64823-23-0.mol

Synonyms:64823-23-0;SCHEMBL377032;3,4-Dimethyl-2-nitrobenzenamine;DTXSID001303758

Suppliers and Price of 3,4-Dimethyl-2-nitroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3,4-Dimethyl-2-nitroaniline

Chemical Property:

Melting Point:63.5 °C
Boiling Point:313.6±37.0 °C(Predicted)
PKA:0.58±0.10(Predicted)
PSA：71.84000
Density:1.220±0.06 g/cm3(Predicted)
LogP:2.89820
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:166.074227566
Heavy Atom Count:12
Complexity:178

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C=C1)N)[N+](=O)[O-])C

Technology Process of 3,4-Dimethyl-2-nitroaniline

There total 12 articles about 3,4-Dimethyl-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.7%

: 74319-98-5
3,4-Dimethyl-2-nitrobenzamid

: 64823-23-0
3,4-Dimethyl-2-nitroanilin

Guidance literature:: With potassium hydroxide; bromine; In water; at 80 ℃; for 2h;
DOI:10.1002/hlca.19800630208

Reference yield:

: 95-64-7
4-amino-o-xylene

: 6972-71-0
4,5-dimethyl-2-nitrobenzenamine

: 64823-22-9
3,4-dimethyl-5-nitro-aniline

: 64823-23-0
3,4-Dimethyl-2-nitroanilin

Guidance literature:

Reference yield:

: 95-64-7
4-amino-o-xylene

: 64823-23-0
3,4-Dimethyl-2-nitroanilin

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 1 h / 0 - 25 °C

2: acetic anhydride; acetic acid; nitric acid / 12 h / 0 - 25 °C

3: hydrogenchloride / water / 4 h / Reflux

With hydrogenchloride; nitric acid; acetic anhydride; acetic acid; triethylamine; In dichloromethane; water;
DOI:10.1039/c6ra12524g