3,4-Dimethyl-2-nitrobenzamid

Base Information

Chemical Name:3,4-Dimethyl-2-nitrobenzamid
CAS No.:74319-98-5
Molecular Formula:C₉H₁₀N₂O₃
Molecular Weight:194.19
Hs Code.:

Synonyms:3,4-Dimethyl-2-nitrobenzamid

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Chemical Property of 3,4-Dimethyl-2-nitrobenzamid

Chemical Property:

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Technology Process of 3,4-Dimethyl-2-nitrobenzamid

There total 3 articles about 3,4-Dimethyl-2-nitrobenzamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 74319-97-4
3,4-Dimethyl-2-nitrobenzoylchlorid

: 74319-98-5
3,4-Dimethyl-2-nitrobenzamid

Guidance literature:: With ammonium carbamate; In benzene; for 2h;
DOI:10.1002/hlca.19800630208

Reference yield:

: 4315-13-3
3,4-Dimethyl-2-nitrobenzoesaeure

: 74319-98-5
3,4-Dimethyl-2-nitrobenzamid

Guidance literature:: Multi-step reaction with 2 steps

1: 85.7 percent / phosphorus pentachloride / benzene / 1.5 h / 40 °C

2: 73 percent / ammonium carbamate / benzene / 2 h

With ammonium carbamate; phosphorus pentachloride; In benzene;
DOI:10.1002/hlca.19800630208

Reference yield:

: 619-04-5
3,4-dimethylbenzoic acid

: 74319-98-5
3,4-Dimethyl-2-nitrobenzamid

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent H₂SO₄, KNO₃ / 1 h / 0 °C

2: 85.7 percent / phosphorus pentachloride / benzene / 1.5 h / 40 °C

3: 73 percent / ammonium carbamate / benzene / 2 h

With ammonium carbamate; phosphorus pentachloride; sulfuric acid; potassium nitrate; In benzene;
DOI:10.1002/hlca.19800630208