Benzenesulfonamide, N-[2-(3-methoxyphenyl)ethyl]-4-methyl-

Base Information

Chemical Name:Benzenesulfonamide, N-[2-(3-methoxyphenyl)ethyl]-4-methyl-
CAS No.:64880-89-3
Molecular Formula:C16H19NO3S
Molecular Weight:305.398
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonamide, N-[2-(3-methoxyphenyl)ethyl]-4-methyl-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenesulfonamide, N-[2-(3-methoxyphenyl)ethyl]-4-methyl-

There total 3 articles about Benzenesulfonamide, N-[2-(3-methoxyphenyl)ethyl]-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 98-59-9
p-toluenesulfonyl chloride

: 2039-67-0
2-(3-methoxyphenyl)-1-ethanamine

: 64880-89-3
N-[(3-methoxyphenyl)ethyl]-4′′-methylbenzenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1021/jo050503t

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 64880-89-3
N-[(3-methoxyphenyl)ethyl]-4′′-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate / toluene / 18 h / Inert atmosphere; Reflux

2: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 6.5 h / Reflux

3: triethylamine / dichloromethane / 6.5 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; boron trifluoride diethyl etherate; ammonium acetate; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/acs.joc.8b02888

Reference yield:

: 3179-09-7,55446-68-9
(E)-1-methoxy-3-(2-nitrovinyl)benzene

: 64880-89-3
N-[(3-methoxyphenyl)ethyl]-4′′-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 6.5 h / Reflux

2: triethylamine / dichloromethane / 6.5 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; boron trifluoride diethyl etherate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.joc.8b02888