N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzaMide

Base Information

Chemical Name:N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzaMide
CAS No.:64950-20-5
Molecular Formula:C9H6Cl4N2O3
Molecular Weight:331.97
Hs Code.:
Mol file:64950-20-5.mol

Synonyms:Benzamide,4-methoxy-N-(1,2,2,2-tetrachloroethyl);N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzamide;N-(1,2,2,2-tetrachloroethyl)-4-methoxybenzamide;

Suppliers and Price of N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-(1,2,2,2-TETRACHLOROETHYL)-4-NITROBENZAMIDE 95.00%
5MG
$ 499.87

Total 2 raw suppliers

Chemical Property of N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzaMide

Chemical Property:

PSA：74.92000
LogP:4.17380

Purity/Quality:

99% ^*data from raw suppliers

N-(1,2,2,2-TETRACHLOROETHYL)-4-NITROBENZAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzaMide

There total 2 articles about N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 63499-62-7
N-(2,2,2-trichloro-1-hydroxyethyl)-4-nitrobenzamide

: 64950-20-5
N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzamide

Guidance literature:: With phosphorus pentachloride; In chloroform; at 20 ℃; for 0.5h;
DOI:10.1016/S0040-4020(01)00434-3

Reference yield:

: 619-80-7
4-nitrobenzamide

: 64950-20-5
N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 90 - 100 °C

2: 86 percent / PCl₅ / CHCl₃ / 0.5 h / 20 °C

With phosphorus pentachloride; In chloroform;
DOI:10.1016/S0040-4020(01)00434-3

Reference yield: 88.0%

: 64950-20-5
N-(1,2,2,2-tetrachloroethyl)-4-nitrobenzamide

: 65432-56-6
N-(2,2-dichlorovinyl)-4-nitrobenzamide

Guidance literature:: With lithium perchlorate; In acetonitrile; at 15 ℃; Electrochemical reaction; cathode - mercury pool, anode - platinum plate, cathodic potential - 0.61 V vs SCE, electricity consumption - 2 F/mol;
DOI:10.1016/S0040-4020(01)00434-3