2-Bromo-3,4-dihydroxy-5-methoxybenzaldehyde

Base Information

Chemical Name:2-Bromo-3,4-dihydroxy-5-methoxybenzaldehyde
CAS No.:65144-12-9
Molecular Formula:C8H7BrO4
Molecular Weight:247.045
Hs Code.:
DSSTox Substance ID:DTXSID30554602
Wikidata:Q82435701

Synonyms:2-Bromo-3,4-dihydroxy-5-methoxybenzaldehyde;65144-12-9;SCHEMBL24140773;DTXSID30554602

Suppliers and Price of 2-Bromo-3,4-dihydroxy-5-methoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Bromo-3,4-dihydroxy-5-methoxybenzaldehyde

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:245.95277
Heavy Atom Count:13
Complexity:187

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C(=C1)C=O)Br)O)O

Technology Process of 2-Bromo-3,4-dihydroxy-5-methoxybenzaldehyde

There total 5 articles about 2-Bromo-3,4-dihydroxy-5-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 3934-87-0
5-hydroxyvanillin

: 65144-12-9
2-bromo-3,4-dihydroxy-5-methoxy-benzaldehyde

Guidance literature:: With bromine; In acetic acid; at 25 ℃; for 16h;
DOI:10.1021/acs.jmedchem.8b00986

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 65144-12-9
2-bromo-3,4-dihydroxy-5-methoxy-benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / acetic acid / 16 h / 25 °C

2: copper / water / 48 h / 100 °C

3: bromine / acetic acid / 16 h / 25 °C

With bromine; copper; In water; acetic acid;
DOI:10.1021/acs.jmedchem.8b00986

Reference yield:

: 2973-76-4
5-bromo-4-hydroxy-3-methoxybenzaldehyde

: 65144-12-9
2-bromo-3,4-dihydroxy-5-methoxy-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: copper / water / 48 h / 100 °C

2: bromine / acetic acid / 16 h / 25 °C

With bromine; copper; In water; acetic acid;
DOI:10.1021/acs.jmedchem.8b00986