2-Quinolinecarboxamide, 6-bromo-

Base Information

• Chemical Name: 2-Quinolinecarboxamide, 6-bromo-
• CAS No.: 65148-09-6
• Molecular Formula: C10H7BrN2O
• Molecular Weight: 251.082
• Hs Code.: 2933499090

Synonyms:6-bromo-5-deazalumazine;6-bromo-quinoline-2-carboxylic acid amide;6-Bromoquinaldonitrile-1-oxide;6-bromopyrido<2,3-d>pyrimidine-2,4-dione;

Chemical Property of 2-Quinolinecarboxamide, 6-bromo-

Chemical Property:

• PSA: 55.98000
• LogP: 2.79650

Purity/Quality:

97% ^*data from raw suppliers

6-Bromo-quinoline-2-carboxylicacidamide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Quinolinecarboxamide, 6-bromo-

There total 5 articles about 2-Quinolinecarboxamide, 6-bromo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

6-Bromo-2-methyl-quinoline (877-42-9) → 6-bromoquinoline-2-carboxamide (65148-09-6)

Guidance literature:

With ammonium acetate; oxygen; copper; In 1,4-dioxane; at 130 ℃; for 36h; under 760.051 Torr; Sealed tube;

DOI:10.1039/c5ob00685f

Reference yield: 72.0%

6-bromoquinoline (5332-25-2) + formamide (77287-34-4,77287-35-5,60100-09-6) → 6-bromoquinoline-2-carboxamide (65148-09-6)

Guidance literature:

With dipotassium peroxodisulfate; at 70 ℃; for 12h; regioselective reaction;

DOI:10.1016/j.tetlet.2017.11.006

Reference yield:

6-bromoquinoline-2-carbonitrile (65185-41-3) → 6-bromoquinoline-2-carboxamide (65148-09-6)

Guidance literature:

With dihydrogen peroxide; potassium carbonate; In acetonitrile; at 20 - 50 ℃; Inert atmosphere;

upstream raw materials:

6-bromoquinoline-2-carbonitrile

6-Bromo-2-methyl-quinoline

6-bromoquinoline

semicarbazide hydrochloride

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