Phosphine oxide, [1-(4-methoxyphenyl)-2-nitroethyl]diphenyl-

Base Information

Chemical Name:Phosphine oxide, [1-(4-methoxyphenyl)-2-nitroethyl]diphenyl-
CAS No.:65164-92-3
Molecular Formula:C21H20NO4P
Molecular Weight:381.368
Hs Code.:

Synonyms:

Suppliers and Price of Phosphine oxide, [1-(4-methoxyphenyl)-2-nitroethyl]diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Phosphine oxide, [1-(4-methoxyphenyl)-2-nitroethyl]diphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Phosphine oxide, [1-(4-methoxyphenyl)-2-nitroethyl]diphenyl-

There total 5 articles about Phosphine oxide, [1-(4-methoxyphenyl)-2-nitroethyl]diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3179-10-0
1-methoxy-4-(2-nitro-vinyl)-benzene

: 4559-70-0
Diphenylphosphine oxide

: 65164-92-3
1-[1-(Diphenyl-phosphinoyl)-2-nitro-ethyl]-4-methoxy-benzene

Guidance literature:: With (1S,2S)-1,2-Cy[NC(Me)CHC(Me)N(2,6-Et₂C₆H₃)]₂YN(SiMe₃)₂; In toluene; at 20 ℃; for 6h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1039/c7ra07565k

Reference yield: 93.0%

: 3179-10-0,5576-97-6
(E)-1-methoxy-4-(2-nitrovinyl)benzene

: 4559-70-0
Diphenylphosphine oxide

: 65164-92-3
1-[1-(Diphenyl-phosphinoyl)-2-nitro-ethyl]-4-methoxy-benzene

Guidance literature:: With η¹:η¹-[η¹:η¹-2-(2,6-ⁱPr₂C₆H₃)N=CH-8-OC₉H₆N]₂LiYb[N(TMS)₂]₂; In tetrahydrofuran; at 20 ℃; for 6h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c5nj00409h

Reference yield: 75.0%

: 3179-10-0,5576-97-6
(E)-1-methoxy-4-(2-nitrovinyl)benzene

: 829-85-6
diphenylphosphane

: 65164-92-3
1-[1-(Diphenyl-phosphinoyl)-2-nitro-ethyl]-4-methoxy-benzene

Guidance literature:: diphenylphosphane; With C₂₄H₂₇ClN₄Ni; sodium acetate; at -20 ℃; for 0.5h;

(E)-1-methoxy-4-(2-nitrovinyl)benzene; at -20 ℃; for 12h;

With dihydrogen peroxide; In water; at 20 ℃; for 2h;
DOI:10.1002/aoc.5954