1(2H)-Isoquinolinone, 2-[(2-bromophenyl)methyl]-3,4-dihydro-

Base Information

Chemical Name:1(2H)-Isoquinolinone, 2-[(2-bromophenyl)methyl]-3,4-dihydro-
CAS No.:65185-66-2
Molecular Formula:C16H14BrNO
Molecular Weight:316.197
Hs Code.:

Synonyms:

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Chemical Property of 1(2H)-Isoquinolinone, 2-[(2-bromophenyl)methyl]-3,4-dihydro-

Chemical Property:

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Technology Process of 1(2H)-Isoquinolinone, 2-[(2-bromophenyl)methyl]-3,4-dihydro-

There total 4 articles about 1(2H)-Isoquinolinone, 2-[(2-bromophenyl)methyl]-3,4-dihydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 414887-25-5
2-(2-bromobenzyl)-1,2,3,4-tetrahydroisoquinoline

: 65185-66-2
2-(2-bromobenzyl)-3,4-dihydroisoquinolin-1(2H)-one

Guidance literature:: With DBN; In acetonitrile; at 20 ℃; for 15h; Schlenk technique; Irradiation;
DOI:10.1002/chem.202100398

Reference yield:

: 119-65-3
isoquinoline

: 65185-66-2
2-(2-bromobenzyl)-3,4-dihydroisoquinolin-1(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: sodium cyanoborohydride; acetic acid / 4 h / 0 - 20 °C

2: sodium carbonate / tetrahydrofuran / 0 - 20 °C

3: DBN / acetonitrile / 15 h / 20 °C / Schlenk technique; Irradiation

With DBN; sodium cyanoborohydride; sodium carbonate; acetic acid; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.202100398

Reference yield:

: 91-21-4
1,2,3,4-tetrahydroisoquinoline

: 3433-80-5
1-Bromo-2-bromomethyl-benzene

: 65185-66-2
2-(2-bromobenzyl)-3,4-dihydroisoquinolin-1(2H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / tetrahydrofuran / 0 - 20 °C

2: DBN / acetonitrile / 15 h / 20 °C / Schlenk technique; Irradiation

With DBN; sodium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.202100398