Butanoyl chloride, 3,3-dimethyl-2-(phenylthio)-

Base Information

• Chemical Name: Butanoyl chloride, 3,3-dimethyl-2-(phenylthio)-
• CAS No.: 65302-96-7
• Molecular Formula: C₁₂H₁₅ClOS
• Molecular Weight: 242.77

Synonyms:

Chemical Property of Butanoyl chloride, 3,3-dimethyl-2-(phenylthio)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Butanoyl chloride, 3,3-dimethyl-2-(phenylthio)-

There total 1 articles about Butanoyl chloride, 3,3-dimethyl-2-(phenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-2-tert-butyl acetic acid (50364-40-4) → 3,3-Dimethyl-2-phenylthiobutanoylchlorid (65302-96-7)

Guidance literature:

With thionyl chloride;

Reference yield:

3,3-Dimethyl-2-phenylthiobutanoylchlorid (65302-96-7) → 1-Acetoxy-4,4-dimethyl-3-phenylthio-2-pentanon (65302-94-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (i), (ii) aq. HCl

2: acetic acid

In acetic acid;

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 3,3-Dimethyl-2-phenylthiobutanoylchlorid (65302-96-7) → 1-Diazo-4,4-dimethyl-3-phenylthio-2-pentanon (69798-57-8)

Guidance literature:

In diethyl ether;

upstream raw materials:

2-bromo-2-tert-butyl acetic acid

Downstream raw materials:

1-Chlor-4,4-dimethyl-3-phenylthio-2-pentanon

1-Diazo-4,4-dimethyl-3-phenylthio-2-pentanon

1-Acetoxy-4,4-dimethyl-3-phenylthio-2-pentanon

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