Cyclopropanecarboxylic acid, 2,2-dimethyl-3-methylene-1-phenyl-, ethyl ester

Base Information

Chemical Name:Cyclopropanecarboxylic acid, 2,2-dimethyl-3-methylene-1-phenyl-, ethyl ester
CAS No.:65354-67-8
Molecular Formula:C15H18O2
Molecular Weight:230.307
Hs Code.:

Synonyms:

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Chemical Property of Cyclopropanecarboxylic acid, 2,2-dimethyl-3-methylene-1-phenyl-, ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Cyclopropanecarboxylic acid, 2,2-dimethyl-3-methylene-1-phenyl-, ethyl ester

There total 3 articles about Cyclopropanecarboxylic acid, 2,2-dimethyl-3-methylene-1-phenyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22065-57-2
ethyl 2-phenyldiazoacetate

: 598-25-4
Dimethylallene

: 65354-67-8
2,2-Dimethyl-3-methylene-1-phenyl-cyclopropanecarboxylic acid ethyl ester

: 65354-73-6
1-Phenyl-2-isopropylidencyclopropancarbonsaeureethylester

Guidance literature:: benzophenone; at -10 ℃; for 0.666667h; Title compound not separated from byproducts; Irradiation;
DOI:10.1021/ja00525a025

Reference yield:

: 1603-79-8
phenylglyoxylic acid ethyl ester

: 65354-67-8
2,2-Dimethyl-3-methylene-1-phenyl-cyclopropanecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 3 h / Ambient temperature

2: HOCH₂CH₂OH, Na / 70 - 75 °C

3: 15 °C / Irradiation

With sodium; ethylene glycol; In methanol;
DOI:10.1021/jo00364a009

Reference yield:

: phenylmagnesium bromide

: 65354-67-8
2,2-Dimethyl-3-methylene-1-phenyl-cyclopropanecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / -78 - 20 °C

2: methanol / 3 h / Ambient temperature

3: HOCH₂CH₂OH, Na / 70 - 75 °C

4: 15 °C / Irradiation

With sodium; ethylene glycol; In methanol; diethyl ether;
DOI:10.1021/jo00364a009