Naphthalene, 2-(1-methylpropyl)-, (S)-

Base Information

Chemical Name:Naphthalene, 2-(1-methylpropyl)-, (S)-
CAS No.:65419-63-8
Molecular Formula:C14H16
Molecular Weight:184.281
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Naphthalene, 2-(1-methylpropyl)-, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Naphthalene, 2-(1-methylpropyl)-, (S)-

There total 20 articles about Naphthalene, 2-(1-methylpropyl)-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1442649-37-7
C₁₆H₁₈O₂S

: 544-97-8
dimethyl zinc(II)

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 65419-63-8
2-(1-Methylpropyl)naphthalene

Guidance literature:: With [nickel(II)dichloride(dimethoxyethane)]; bis[2-(diphenylphosphino)phenyl] ether; In toluene; at 20 ℃; for 24h; enantiospecific reaction; Inert atmosphere;
DOI:10.1021/ja4034999

Reference yield:

: 66-99-9
β-naphthaldehyde

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 65419-63-8
2-(1-Methylpropyl)naphthalene

Guidance literature:: Multi-step reaction with 3 steps

1.1: (R)-1,1'-Bi-2-naphthol; titanium(IV) isopropylate / hexane; dichloromethane / 0.17 h / 20 °C / Inert atmosphere

1.2: 15 h / 0 °C / Inert atmosphere

2.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere

3.1: [nickel(II)dichloride(dimethoxyethane)]; bis[2-(diphenylphosphino)phenyl] ether / toluene / 24 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; dmap; [nickel(II)dichloride(dimethoxyethane)]; (R)-1,1'-Bi-2-naphthol; dicyclohexyl-carbodiimide; bis[2-(diphenylphosphino)phenyl] ether; In hexane; dichloromethane; toluene; 3.1: |Negishi Coupling;
DOI:10.1021/ja4034999

Reference yield:

: 87241-23-4,132154-59-7,112576-12-2
(R)-1-(2-naphthyl)propanol

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 65419-63-8
2-(1-Methylpropyl)naphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere

2: [nickel(II)dichloride(dimethoxyethane)]; bis[2-(diphenylphosphino)phenyl] ether / toluene / 24 h / 20 °C / Inert atmosphere

With dmap; [nickel(II)dichloride(dimethoxyethane)]; dicyclohexyl-carbodiimide; bis[2-(diphenylphosphino)phenyl] ether; In dichloromethane; toluene; 2: |Negishi Coupling;
DOI:10.1021/ja4034999