DIETHYL 3-METHOXYPHENYLPHOSPHONATE

Base Information

Chemical Name:DIETHYL 3-METHOXYPHENYLPHOSPHONATE
CAS No.:65442-22-0
Molecular Formula:C11H17O4P
Molecular Weight:244.227
Hs Code.:
Mol file:65442-22-0.mol

Synonyms:diethyl 3-methoxyphenylphosphonate;3-Anisylphosphonsaeurediethylester;diethyl (3-methoxyphenyl)phosphate;diethyl 3-anizylphosphonate;O,O-Diethyl-m-methoxyphenylphosphonat;diethyl (3-methoxyphenyl)phosphonate;

Suppliers and Price of DIETHYL 3-METHOXYPHENYLPHOSPHONATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of DIETHYL 3-METHOXYPHENYLPHOSPHONATE

Chemical Property:

PSA：54.57000
LogP:2.58660

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of DIETHYL 3-METHOXYPHENYLPHOSPHONATE

There total 20 articles about DIETHYL 3-METHOXYPHENYLPHOSPHONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2398-37-0
3-methoxyphenyl bromide

: 122-52-1
triethyl phosphite

: 65442-22-0
(3-methoxyphenyl)phosphonic acid diethyl ester

Guidance literature:: With nickel dichloride; for 0.0833333h; Microwave irradiation;
DOI:10.1016/j.cclet.2010.01.030

Reference yield: 88.0%

: 53392-03-3
(3-methoxyphenyl)triethoxysilane

: 762-04-9
phosphonic acid diethyl ester

: 65442-22-0
(3-methoxyphenyl)phosphonic acid diethyl ester

Guidance literature:: (3-methoxyphenyl)triethoxysilane; With bis-triphenylphosphine-palladium(II) chloride; potassium fluoride; silver carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h; Sealed tube;

phosphonic acid diethyl ester; In N,N-dimethyl-formamide; at 80 ℃; for 12h; Sealed tube;
DOI:10.1039/C6CC08408G

Reference yield: 88.0%

: 1-(3-methoxybenzoyl)piperidine-2,6-dione

: 762-04-9
phosphonic acid diethyl ester

: 65442-22-0
(3-methoxyphenyl)phosphonic acid diethyl ester

Guidance literature:: With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); sodium carbonate; In 1,4-dioxane; at 160 ℃; for 15h; Reagent/catalyst; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201707102