2-(p-Tolyl)-1,3-dioxolane

Base Information

Chemical Name:2-(p-Tolyl)-1,3-dioxolane
CAS No.:2403-51-2
Molecular Formula:C10H12 O2
Molecular Weight:164.204
Hs Code.:
DSSTox Substance ID:DTXSID401302940
Nikkaji Number:J145.050F
Mol file:2403-51-2.mol

Synonyms:2403-51-2;2-(p-Tolyl)-1,3-dioxolane;2-(4-methylphenyl)-1,3-dioxolane;2-p-tolyl-1,3-dioxolane;SCHEMBL8363106;DTXSID401302940;AKOS006295792

Suppliers and Price of 2-(p-Tolyl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-(p-Tolyl)-1,3-dioxolane

Chemical Property:

Vapor Pressure:0.0245mmHg at 25°C
Boiling Point:256.6°C at 760 mmHg
Flash Point:112.1°C
PSA：18.46000
Density:1.085g/cm³
LogP:2.04040
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:164.083729621
Heavy Atom Count:12
Complexity:133

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2OCCO2

Technology Process of 2-(p-Tolyl)-1,3-dioxolane

There total 11 articles about 2-(p-Tolyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 104-87-0
4-methyl-benzaldehyde

: 107-21-1
ethylene glycol

: 2403-51-2
2-(4-methylphenyl)-1,3-dioxolane

Guidance literature:: With Eosin Y; In acetonitrile; at 20 ℃; for 12h; chemoselective reaction; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.6b03403

Reference yield: 86.0%

: 10602-01-4
p-bromobenzaldehyde 1,3-dioxolane

: 917-54-4
methyllithium

: 2403-51-2
2-(4-methylphenyl)-1,3-dioxolane

Guidance literature:: p-bromobenzaldehyde 1,3-dioxolane; With bis(tri-t-butylphosphine)palladium⁽⁰⁾; oxygen; In toluene; at 20 ℃; for 0.0166667h; Schlenk technique;

methyllithium; In toluene; at 20 ℃; for 0.0333333h; Schlenk technique;
DOI:10.1002/anie.201700417