butane-1,4-diyl disulfamate

Base Information

• Chemical Name: butane-1,4-diyl disulfamate
• CAS No.: 60548-62-1
• Molecular Formula: C4H12N2O6S2
• Molecular Weight: 248.30
• Mol file: 60548-62-1.mol

Synonyms:

Chemical Property of butane-1,4-diyl disulfamate

Chemical Property:

• Vapor Pressure: 9.21E-09mmHg at 25°C
• Boiling Point: 463.3°Cat760mmHg
• Flash Point: 234°C
• Density: 1.584g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of butane-1,4-diyl disulfamate

There total 2 articles about butane-1,4-diyl disulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Butane-1,4-diol (110-63-4) → 1,4-butanediyl sulfamate (60548-62-1)

Guidance literature:

With sulphamoyl chloride; sodium hydride; Yield given. Multistep reaction; 1.) 1,2-dimethoxyethane, RT, 2 h, 2.) 1,2-dimethoxyethane, 4 deg C, 24 h;

DOI:10.1021/jm00139a029

Reference yield:

→ 1,4-butanediyl sulfamate (60548-62-1)

Guidance literature:

Diol, Chlorsulfonamid;

upstream raw materials:

Butane-1,4-diol

Refernces

• 1、 Hirsch, Allen F.,Kasulanis, Charles,Kraft, Larry,Mallory, Robert A.,Powell, Gregory,Wong, Benny. "Synthesis and Evaluation of the Male Antifertility Properties of a Series of N-Unsubstituted Sulfamates". . p. 901 - 903. Retrieved 2007/10/02.