1,4-Butanedione, 4-(4-chlorophenyl)-1,2-diphenyl-

Base Information

Chemical Name:1,4-Butanedione, 4-(4-chlorophenyl)-1,2-diphenyl-
CAS No.:65690-99-5
Molecular Formula:C22H17ClO2
Molecular Weight:348.829
Hs Code.:
DSSTox Substance ID:DTXSID90462471
Nikkaji Number:J2.024.238H

Synonyms:1,4-Butanedione, 4-(4-chlorophenyl)-1,2-diphenyl-;65690-99-5;SCHEMBL11520271;DTXSID90462471;LXWRMHZVTZOYTG-UHFFFAOYSA-N;1,2-diphenyl4-p-chlorophenylbutane-1,4-dione;1,2-Diphenyl-4-(4-chlorophenyl)butane-1,4-dione

Suppliers and Price of 1,4-Butanedione, 4-(4-chlorophenyl)-1,2-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,4-Butanedione, 4-(4-chlorophenyl)-1,2-diphenyl-

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:348.0917075
Heavy Atom Count:25
Complexity:441

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(CC(=O)C2=CC=C(C=C2)Cl)C(=O)C3=CC=CC=C3

Technology Process of 1,4-Butanedione, 4-(4-chlorophenyl)-1,2-diphenyl-

There total 4 articles about 1,4-Butanedione, 4-(4-chlorophenyl)-1,2-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 5908-41-8
benzoyltrimethylsilane

: 22966-22-9
(E)-1-(4-chlorophenyl)-3-phenyl-2-propen-1-one

: 65690-99-5
4‐(4‐chlorophenyl)‐1,2‐diphenylbutane‐1,4‐dione

Guidance literature:: With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; isopropyl alcohol; In tetrahydrofuran; at 70 ℃; for 24h;
DOI:10.1021/ja0318380

Reference yield: 78.0%

: 3923-51-1
1,1-diphenylprop-2-en-1-ol

: 104-88-1
4-chlorobenzaldehyde

: 65690-99-5
4‐(4‐chlorophenyl)‐1,2‐diphenylbutane‐1,4‐dione

Guidance literature:: With tert-Butyl peroxybenzoate; In toluene; for 24h; Heating;
DOI:10.1002/aoc.4407

Reference yield: 68.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: C₁₆H₁₂ClNO₃

: 100-52-7
benzaldehyde

: 65690-99-5
4‐(4‐chlorophenyl)‐1,2‐diphenylbutane‐1,4‐dione

Guidance literature:: With 3-mesityl-4,5,6,7-tetrahydrobenzo[d]thiazol-3-ium perchlorate; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 65 ℃; for 16h; regioselective reaction; Irradiation;
DOI:10.1021/acscatal.1c04594