2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-[(dimethylamino)carbonyl]- 1H-1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-a-(phenylmethyl)-, (S)-

Base Information

Chemical Name:2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-[(dimethylamino)carbonyl]- 1H-1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-a-(phenylmethyl)-, (S)-
CAS No.:65699-23-2
Molecular Formula:C₃₆H₂₈Cl₂N₆O₅
Molecular Weight:695.562
Hs Code.:

2H-Isoindole-2-acetamide,
N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-[(dimethylamino)carbonyl]-
1H-1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-a-(phenylmethyl)-,
(S)-

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Chemical Property of 2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-[(dimethylamino)carbonyl]- 1H-1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-a-(phenylmethyl)-, (S)-

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Technology Process of 2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-[(dimethylamino)carbonyl]- 1H-1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-a-(phenylmethyl)-, (S)-

There total 7 articles about 2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-[(dimethylamino)carbonyl]- 1H-1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-a-(phenylmethyl)-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50330-59-1
8-chloro-6-(2-chloro-phenyl)-4H-benzo[f][1,2,4]triazolo[1,5-a][1,4]diazepine-2-carboxylic acid dimethylamide

: 65699-23-2
2',5-dichloro-2-(3-dimethylcarbamoyl-5-phthalylphenylalanylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HBr / Heating

2: benzene; dimethylformamide / 4 h / Ambient temperature

With hydrogen bromide; In N,N-dimethyl-formamide; benzene;
DOI:10.1002/jhet.5570190621

Reference yield:

: 65698-99-9
N,N-dimethyl 2-amino-2-(2-(2-chlorobenzoyl)-5-chlorophenylazo)acetamide

: 65699-23-2
2',5-dichloro-2-(3-dimethylcarbamoyl-5-phthalylphenylalanylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / K₂CO₃ / tetrahydrofuran; dimethylformamide / Ambient temperature; overnight

2: 30percent HBr/acetic acid / 2 h / Ambient temperature

3: benzene; dimethylformamide / 4 h / Ambient temperature

With hydrogen bromide; potassium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; benzene;
DOI:10.1002/jhet.5570190621

Reference yield:

: 65698-98-8
C₁₇H₁₅Cl₂N₃O₃

: 65699-23-2
2',5-dichloro-2-(3-dimethylcarbamoyl-5-phthalylphenylalanylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / methanol / 96 h / Ambient temperature

2: 47 percent / K₂CO₃ / tetrahydrofuran; dimethylformamide / Ambient temperature; overnight

3: 30percent HBr/acetic acid / 2 h / Ambient temperature

4: benzene; dimethylformamide / 4 h / Ambient temperature

With hydrogen bromide; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; benzene;
DOI:10.1002/jhet.5570190621