Phosphonic acid, [1-(3-methylphenyl)ethyl]-, diethyl ester

Base Information

Chemical Name:Phosphonic acid, [1-(3-methylphenyl)ethyl]-, diethyl ester
CAS No.:65797-29-7
Molecular Formula:C13H21O3P
Molecular Weight:256.282
Hs Code.:

Synonyms:

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Chemical Property of Phosphonic acid, [1-(3-methylphenyl)ethyl]-, diethyl ester

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Technology Process of Phosphonic acid, [1-(3-methylphenyl)ethyl]-, diethyl ester

There total 5 articles about Phosphonic acid, [1-(3-methylphenyl)ethyl]-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: diethyl (1-(m-tolyl)vinyl)phosphonate

: 65797-29-7
diethyl (1-(m-tolyl)ethyl)phosphonate

Guidance literature:: With potassium phosphate; 2-nitrobenzenesulfonyl hydrazide; In acetonitrile; at 20 ℃; for 5h; chemoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2016.02.057

Reference yield:

: 1309980-37-7
diethyl 1-[(4-methylbenzenesulfonyl)oxy]ethene-alpha-phosphonate

: 65797-29-7
diethyl (1-(m-tolyl)ethyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; palladium diacetate / toluene / 20 °C

2: ammonium formate; palladium 10% on activated carbon / methanol / Inert atmosphere

With palladium 10% on activated carbon; ammonium formate; palladium diacetate; caesium carbonate; In methanol; toluene; 1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol503518h

Reference yield:

: 919-19-7
diethyl acetylphosphonate

: 65797-29-7
diethyl (1-(m-tolyl)ethyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile

2: caesium carbonate; palladium diacetate / toluene / 20 °C

3: ammonium formate; palladium 10% on activated carbon / methanol / Inert atmosphere

With palladium 10% on activated carbon; ammonium formate; palladium diacetate; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; toluene; acetonitrile; 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol503518h