1,1-Dimethoxy-2-methylidenecyclohexane

Base Information

• Chemical Name: 1,1-Dimethoxy-2-methylidenecyclohexane
• CAS No.: 65818-17-9
• Molecular Formula: C9H16O2
• Molecular Weight: 156.225
• DSSTox Substance ID: DTXSID80493173
• Wikidata: Q82339681

Synonyms:1,1-Dimethoxy-2-methylidenecyclohexane;65818-17-9;DTXSID80493173

Chemical Property of 1,1-Dimethoxy-2-methylidenecyclohexane

Chemical Property:

• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 156.115029749
• Heavy Atom Count: 11
• Complexity: 148

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1(CCCCC1=C)OC

Technology Process of 1,1-Dimethoxy-2-methylidenecyclohexane

There total 2 articles about 1,1-Dimethoxy-2-methylidenecyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dimethoxycyclohexanone (38461-13-1) + Methyltriphenylphosphonium bromide (1779-49-3) → dimethoxy-2,2 methylenecyclohexane (65818-17-9)

Guidance literature:

With sodium tert-pentoxide; Yield given. Multistep reaction; 1.) benzene, 30 min, RT, 2.) benzene, 6 h, reflux;

Reference yield:

2,2-dimethoxycyclohexanone (38461-13-1) + Methylenetriphenylphosphorane (19493-09-5) → dimethoxy-2,2 methylenecyclohexane (65818-17-9)

Guidance literature:

DOI:10.1016/S0040-4039(01)83278-0

Reference yield: 90.0%

dimethoxy-2,2 methylenecyclohexane (65818-17-9) → 2-methylenecyclohexanone (3045-98-5)

Guidance literature:

With oxalic acid; silica gel; In chloroform; for 0.5h; Ambient temperature;

upstream raw materials:

2,2-dimethoxycyclohexanone

Methylenetriphenylphosphorane

Methyltriphenylphosphonium bromide

Downstream raw materials:

2-methylenecyclohexanone

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