Acetic acid, [[2-[4-(aminosulfonyl)phenyl]-6,7-dichloro-2,3-dihydro-2-methyl-1-oxo-1 H-inden-5-yl]oxy]-

Base Information

Chemical Name:Acetic acid, [[2-[4-(aminosulfonyl)phenyl]-6,7-dichloro-2,3-dihydro-2-methyl-1-oxo-1 H-inden-5-yl]oxy]-
CAS No.:66015-32-5
Molecular Formula:C18H15Cl2NO6S
Molecular Weight:444.292
Hs Code.:

Synonyms:

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Chemical Property of Acetic acid, [[2-[4-(aminosulfonyl)phenyl]-6,7-dichloro-2,3-dihydro-2-methyl-1-oxo-1 H-inden-5-yl]oxy]-

Chemical Property:

Purity/Quality:

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Technology Process of Acetic acid, [[2-[4-(aminosulfonyl)phenyl]-6,7-dichloro-2,3-dihydro-2-methyl-1-oxo-1 H-inden-5-yl]oxy]-

There total 18 articles about Acetic acid, [[2-[4-(aminosulfonyl)phenyl]-6,7-dichloro-2,3-dihydro-2-methyl-1-oxo-1 H-inden-5-yl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66015-59-6
[1-Oxo-2-(4-chlorosulfonylphenyl)-2-methyl-6,7-dichloro-5-indanyloxy]acetic acid

: 66015-32-5
[1-oxo-2-methyl-2-(4-sulfamoylphenyl)-6,7-dichloro-5-indanyloxy]acetic acid

Guidance literature:: With ammonia; In water;

Reference yield:

: 1984-59-4
2,3-dichloroanisole

: 66015-32-5
[1-oxo-2-methyl-2-(4-sulfamoylphenyl)-6,7-dichloro-5-indanyloxy]acetic acid

Guidance literature:: Multi-step reaction with 10 steps

1: aluminium trichloride / dichloromethane

2: bromine; sodium hydrogensulfite / acetic acid

3: lithium bromide / N,N-dimethyl-formamide

4: (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid

5: potassium tert-butylate / water; tert-butyl alcohol

6: pyridine hydrochloride

7: potassium iodide; potassium carbonate / acetone

8: sulfuric acid; acetic acid / water

9: chlorosulfonic acid

10: ammonia / water

With chlorosulfonic acid; lithium bromide; potassium iodide; sulfuric acid; potassium tert-butylate; ammonia; bromine; pyridine hydrochloride; potassium carbonate; sodium hydrogensulfite; acetic acid; aluminium trichloride; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; dichloromethane; sulfuric acid; water; acetic acid; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;

Reference yield:

: 53107-35-0
2',3',-Dichloro-4'-methoxyisobutyrophenone

: 66015-32-5
[1-oxo-2-methyl-2-(4-sulfamoylphenyl)-6,7-dichloro-5-indanyloxy]acetic acid

Guidance literature:: Multi-step reaction with 8 steps

1: bromine; sodium hydrogensulfite / acetic acid

2: lithium bromide / N,N-dimethyl-formamide

3: (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid

4: potassium tert-butylate / water; tert-butyl alcohol

5: pyridine hydrochloride

6: sodium hydrogencarbonate / 1,2-dimethoxyethane; ethanol; water

7: chlorosulfonic acid

8: ammonia / water

With chlorosulfonic acid; lithium bromide; potassium tert-butylate; ammonia; bromine; pyridine hydrochloride; sodium hydrogencarbonate; sodium hydrogensulfite; In 1,2-dimethoxyethane; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; ethanol; sulfuric acid; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;