Technology Process of Acetic acid,
[[6,7-dichloro-2-[4-(chlorosulfonyl)phenyl]-2,3-dihydro-2-methyl-1-oxo-1
H-inden-5-yl]oxy]-
There total 17 articles about Acetic acid,
[[6,7-dichloro-2-[4-(chlorosulfonyl)phenyl]-2,3-dihydro-2-methyl-1-oxo-1
H-inden-5-yl]oxy]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chlorosulfonic acid;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: aluminium trichloride / dichloromethane
2: bromine; sodium hydrogensulfite / acetic acid
3: lithium bromide / N,N-dimethyl-formamide
4: (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid
5: potassium tert-butylate / water; tert-butyl alcohol
6: pyridine hydrochloride
7: sodium hydrogencarbonate / 1,2-dimethoxyethane; ethanol; water
8: chlorosulfonic acid
With
chlorosulfonic acid; lithium bromide; potassium tert-butylate; bromine; pyridine hydrochloride; sodium hydrogencarbonate; sodium hydrogensulfite;
aluminium trichloride;
In
1,2-dimethoxyethane; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; ethanol; dichloromethane; sulfuric acid; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: bromine; sodium hydrogensulfite / acetic acid
2: lithium bromide / N,N-dimethyl-formamide
3: (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid
4: potassium tert-butylate / water; tert-butyl alcohol
5: pyridine hydrochloride
6: potassium hydroxide; potassium carbonate / N-methyl-acetamide; methanol; water
7: chlorosulfonic acid
With
chlorosulfonic acid; potassium hydroxide; lithium bromide; potassium tert-butylate; bromine; pyridine hydrochloride; potassium carbonate; sodium hydrogensulfite;
In
N-methyl-acetamide; methanol; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;
