4(1H)-Pyrimidinone, 2,3-dihydro-5-(3-methylphenoxy)-2-thioxo-

Base Information

• Chemical Name: 4(1H)-Pyrimidinone, 2,3-dihydro-5-(3-methylphenoxy)-2-thioxo-
• CAS No.: 66047-03-8
• Molecular Formula: C11H10N2O2S
• Molecular Weight: 234.27400
• Mol file: 66047-03-8.mol

Synonyms:2-Mercapto-5-m-tolyloxy-pyrimidin-4-ol;5-m-Tolyloxy-2-thio-uracil;

Chemical Property of 4(1H)-Pyrimidinone, 2,3-dihydro-5-(3-methylphenoxy)-2-thioxo-

Chemical Property:

• Melting Point: 215 - 216 °C
• PSA: 94.04000
• LogP: 2.57160

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4(1H)-Pyrimidinone, 2,3-dihydro-5-(3-methylphenoxy)-2-thioxo-

There total 1 articles about 4(1H)-Pyrimidinone, 2,3-dihydro-5-(3-methylphenoxy)-2-thioxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-thioxo-5-m-tolyloxy-2,3-dihydro-1H-pyrimidin-4-one (66047-03-8)

Guidance literature:

/BRN= 227177/;

DOI:10.1021/ja01153a515

Reference yield: 92.0%

2-thioxo-5-m-tolyloxy-2,3-dihydro-1H-pyrimidin-4-one (66047-03-8) → 5-(m-tolyloxy)pyrimidine-2,4(1H,3H)-dione (66047-04-9)

Guidance literature:

With hydrogenchloride; chloroacetic acid;

DOI:10.1021/jm00183a012

Reference yield: 54.0%

2-thioxo-5-m-tolyloxy-2,3-dihydro-1H-pyrimidin-4-one (66047-03-8) → 5-m-Tolyloxy-3H-pyrimidin-4-one

Guidance literature:

With sodium hydroxide; nickel; In water; for 2h; Heating;

DOI:10.1021/jm00183a012

Downstream raw materials:

5-(m-tolyloxy)pyrimidine-2,4(1H,3H)-dione