2-chloro-N,N-diphenylbenzamide

Base Information

Chemical Name:2-chloro-N,N-diphenylbenzamide
CAS No.:66087-68-1
Molecular Formula:C19H14ClNO
Molecular Weight:307.779
Hs Code.:
DSSTox Substance ID:DTXSID00391521
Wikidata:Q82189027

Synonyms:2-chloro-N,N-diphenylbenzamide;66087-68-1;Benzamide, 2-chloro-N,N-diphenyl-;SCHEMBL8075339;DTXSID00391521

Suppliers and Price of 2-chloro-N,N-diphenylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-chloro-N,N-diphenylbenzamide

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:307.0763918
Heavy Atom Count:22
Complexity:342

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N(C2=CC=CC=C2)C(=O)C3=CC=CC=C3Cl

Technology Process of 2-chloro-N,N-diphenylbenzamide

There total 7 articles about 2-chloro-N,N-diphenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.4%

: 609-65-4
o-chlorobenzoyl chloride

: 122-39-4
diphenylamine

: 66087-68-1
2-chloro-N,N-diphenylbenzamide

Guidance literature:: With pyridine; In dichloromethane; at 35 - 45 ℃;

Reference yield: 60.0%

: 591-50-4
iodobenzene

: 6833-13-2
2-chlorobenzanilide

: 66087-68-1
2-chloro-N,N-diphenylbenzamide

Guidance literature:: With potassium phosphate; copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; In toluene; at 130 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol200750p

Reference yield:

: 609-65-4
o-chlorobenzoyl chloride

: 62-53-3
aniline

: 66087-68-1
2-chloro-N,N-diphenylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / dichloromethane / 15 h / 0 - 40 °C / Inert atmosphere

2: copper(l) iodide; potassium phosphate; 2,2,6,6-tetramethylheptane-3,5-dione / toluene / 24 h / 130 °C / Inert atmosphere

With pyridine; dmap; potassium phosphate; copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; In dichloromethane; toluene;
DOI:10.1021/ol200750p