N-[2-(Prop-2-en-1-yl)phenyl]methanesulfonamide

Base Information

Chemical Name:N-[2-(Prop-2-en-1-yl)phenyl]methanesulfonamide
CAS No.:66236-13-3
Molecular Formula:C10H13NO2S
Molecular Weight:211.285
Hs Code.:
DSSTox Substance ID:DTXSID00496464
Nikkaji Number:J3.148.267D

Synonyms:66236-13-3;N-[2-(Prop-2-en-1-yl)phenyl]methanesulfonamide;N-methylsulfonyl-2-allylaniline;SCHEMBL8420054;DTXSID00496464

Suppliers and Price of N-[2-(Prop-2-en-1-yl)phenyl]methanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-[2-(Prop-2-en-1-yl)phenyl]methanesulfonamide

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:211.06669983
Heavy Atom Count:14
Complexity:279

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CS(=O)(=O)NC1=CC=CC=C1CC=C

Technology Process of N-[2-(Prop-2-en-1-yl)phenyl]methanesulfonamide

There total 4 articles about N-[2-(Prop-2-en-1-yl)phenyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 32704-22-6
2-allyl-phenylamine

: 124-63-0
methanesulfonyl chloride

: 66236-13-3
N-(2-allyl-phenyl)-methyl-sulfonamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; Sealed tube; Inert atmosphere;
DOI:10.1021/jo402705w

Reference yield:

: 62-53-3
aniline

: 66236-13-3
N-(2-allyl-phenyl)-methyl-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 70 °C

2: boron trifluoride diethyl etherate / xylenes / 6 h / 180 °C

3: pyridine / dichloromethane / 24 h / 20 °C

With pyridine; boron trifluoride diethyl etherate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; xylenes; 2: Aza-Claisen rearrangement;
DOI:10.1021/ja211272v

Reference yield:

: 589-09-3
N-allyl-N-phenylamine

: 66236-13-3
N-(2-allyl-phenyl)-methyl-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / xylenes / 6 h / 180 °C

2: pyridine / dichloromethane / 24 h / 20 °C

With pyridine; boron trifluoride diethyl etherate; In dichloromethane; xylenes; 1: Aza-Claisen rearrangement;
DOI:10.1021/ja211272v