4,5-Bis[(trimethylsilyl)oxy]-1,4-cyclohexadiene-1,2-dicarboxylic acid dimethyl ester

Base Information

Chemical Name:4,5-Bis[(trimethylsilyl)oxy]-1,4-cyclohexadiene-1,2-dicarboxylic acid dimethyl ester
CAS No.:66322-98-3
Molecular Formula:C16H28O6Si2
Molecular Weight:372.566
Hs Code.:2931900090
Mol file:66322-98-3.mol

Synonyms:dimethyl 4,5-bis(trimethylsilyloxy)cyclohexa-1,4-diene-1,2-dicarboxylate;dimethyl 4,5-bis((trimethylsilyl)oxy)cyclohexa-1,4-dienedicarboxylate;4,5-bis(trimethylsilyloxy)-1,4-cyclohexadiene-1,2-dicarboxylic acid dimethyl ester;4,5-bis(trimethylsilyloxy)cyclohexa-1,4-diene-1,2-dicarboxylic acid dimethyl ester;

Suppliers and Price of 4,5-Bis[(trimethylsilyl)oxy]-1,4-cyclohexadiene-1,2-dicarboxylic acid dimethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,5-Bis[(trimethylsilyl)oxy]-1,4-cyclohexadiene-1,2-dicarboxylic acid dimethyl ester

Chemical Property:

PSA：71.06000
LogP:3.33740

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of 4,5-Bis[(trimethylsilyl)oxy]-1,4-cyclohexadiene-1,2-dicarboxylic acid dimethyl ester

There total 2 articles about 4,5-Bis[(trimethylsilyl)oxy]-1,4-cyclohexadiene-1,2-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.6%

: 31411-71-9
2,3-bis(trimethylsilyloxy)-1,3-butadiene

: 762-42-5
dimethyl acetylenedicarboxylate

: 66322-98-3
1,2-bis(trimethylsilyloxy)-1,4-cyclohexadiene-4,5-dicarboxylic acid dimethyl ester

Guidance literature:: at 90 ℃; for 24h;
DOI:10.1021/jo9919254

Reference yield:

: 17082-61-0
1,2-bis(trimethylsiloxy)cyclobutene

: 66322-98-3
1,2-bis(trimethylsilyloxy)-1,4-cyclohexadiene-4,5-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: benzene-1,4-diol

2: toluene / Heating

With hydroquinone; In toluene;
DOI:10.1021/jo00407a048