Benzeneethanol, 2-iodo-b-methyl-

Base Information

Chemical Name:Benzeneethanol, 2-iodo-b-methyl-
CAS No.:66386-66-1
Molecular Formula:C9H11IO
Molecular Weight:262.09
Hs Code.:

Synonyms:

Suppliers and Price of Benzeneethanol, 2-iodo-b-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Benzeneethanol, 2-iodo-b-methyl-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzeneethanol, 2-iodo-b-methyl-

There total 6 articles about Benzeneethanol, 2-iodo-b-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61161-21-5
2-(1'-methylethenyl)-1-iodobenzene

: 66386-66-1
2-(2-iodophenyl)propan-1-ol

Guidance literature:: 2-(1'-methylethenyl)-1-iodobenzene; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol8008792

Reference yield:

: 33994-46-6
2-(2-iodophenyl)propanoic acid

: 66386-66-1
2-(2-iodophenyl)propan-1-ol

Guidance literature:: 2-(2-iodophenyl)propanoic acid; With sodium tetrahydroborate; In tetrahydrofuran; at 0 ℃; for 0.333333h; Sealed tube; Inert atmosphere;

With boron trifluoride diethyl etherate; In tetrahydrofuran; at 0 - 20 ℃; for 16h; Sealed tube; Inert atmosphere;
DOI:10.1002/chem.201703527

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 66386-66-1
2-(2-iodophenyl)propan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid

2.1: diethyl ether / 3.5 h / 0 - 20 °C / Inert atmosphere

2.2: Cooling with ice

3.1: toluene-4-sulfonic acid; hydroquinone / benzene / Reflux; Azeotropic water removal

4.1: dimethylsulfide borane complex / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

4.2: 1 h / 20 - 40 °C

4.3: 20 - 30 °C

With dimethylsulfide borane complex; sulfuric acid; toluene-4-sulfonic acid; hydroquinone; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1016/j.tetasy.2011.03.012