(2,6-Dimethoxyphenyl)(diphenyl)phosphane

Base Information

Chemical Name:(2,6-Dimethoxyphenyl)(diphenyl)phosphane
CAS No.:66417-43-4
Molecular Formula:C20H19O2P
Molecular Weight:322.343
Hs Code.:
DSSTox Substance ID:DTXSID10514269
Nikkaji Number:J1.105.804C
Wikidata:Q82374487

Synonyms:(2,6-Dimethoxyphenyl)(diphenyl)phosphane;66417-43-4;SCHEMBL17529705;DTXSID10514269

Suppliers and Price of (2,6-Dimethoxyphenyl)(diphenyl)phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of (2,6-Dimethoxyphenyl)(diphenyl)phosphane

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:322.11226684
Heavy Atom Count:23
Complexity:307

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=CC=C1)OC)P(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of (2,6-Dimethoxyphenyl)(diphenyl)phosphane

There total 2 articles about (2,6-Dimethoxyphenyl)(diphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 151-10-0
1,3-Dimethoxybenzene

: 66417-43-4
(2,6-dimethoxyphenyl)diphenylphosphine

Guidance literature:: 1,3-Dimethoxybenzene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; diethyl ether; at 0 ℃; for 1.5h; Inert atmosphere; Schlenk technique;

chloro-diphenylphosphine; In tetrahydrofuran; diethyl ether; at -50 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3cc47700b

Reference yield:

: 2785-97-9
(2,6-dimethoxyphenyl)lithium

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 66417-43-4
(2,6-dimethoxyphenyl)diphenylphosphine

Guidance literature:: DOI:10.1039/c39840000482

Reference yield: 96.0%

: 14873-63-3,15617-19-3,51921-56-3
bis(benzonitrile)dichloroplatinum(II)

: 66417-43-4
(2,6-dimethoxyphenyl)diphenylphosphine

: 67108-69-4
trans-dichlorobis(2,6-dimethoxyphenyldiphenylphosphine)platinum(II)

Guidance literature:: In dichloromethane; Ar-atmosphere; addn. of 2.2 equiv. of phosphine to soln. of Pt-complex; crystn. on MeOH addn.; elem. anal.;
DOI:10.1039/DT9780000257