2-Propenamide, 2-nitro-3-phenyl-N-(phenylmethyl)-

Base Information

Chemical Name:2-Propenamide, 2-nitro-3-phenyl-N-(phenylmethyl)-
CAS No.:666705-44-8
Molecular Formula:C16H14N2O3
Molecular Weight:282.299
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propenamide, 2-nitro-3-phenyl-N-(phenylmethyl)-

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Technology Process of 2-Propenamide, 2-nitro-3-phenyl-N-(phenylmethyl)-

There total 3 articles about 2-Propenamide, 2-nitro-3-phenyl-N-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 129222-48-6
N-benzyl-2-nitroacetamide

: 100-52-7
benzaldehyde

: 666705-44-8
N-benzyl-2-nitro-3-phenylacrylamide

Guidance literature:: With 4-methyl-morpholine; titanium tetrachloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol036461h

Reference yield:

: 2564-06-9
N-benzyl-2-chloroacetamide

: 666705-44-8
N-benzyl-2-nitro-3-phenylacrylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / sodium iodide / acetone / 7 h / 20 °C

2: 84 percent / silver(I) nitrate / tetrahydrofuran; diethyl ether / 18 h / 20 °C

3: 58 percent / TiCl₄; N-methyl morpholine / tetrahydrofuran; CH₂Cl₂

With 4-methyl-morpholine; titanium tetrachloride; silver nitrate; sodium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; 3: Knoevenagel condensation;
DOI:10.1021/ol036461h

Reference yield:

: 64297-96-7
N-(iodoacetyl)benzylamine

: 666705-44-8
N-benzyl-2-nitro-3-phenylacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / silver(I) nitrate / tetrahydrofuran; diethyl ether / 18 h / 20 °C

2: 58 percent / TiCl₄; N-methyl morpholine / tetrahydrofuran; CH₂Cl₂

With 4-methyl-morpholine; titanium tetrachloride; silver nitrate; In tetrahydrofuran; diethyl ether; dichloromethane; 2: Knoevenagel condensation;
DOI:10.1021/ol036461h