Technology Process of Benzenamine,
4,4'-[(5-ethenyl-1,3-phenylene)di-2,1-ethenediyl]bis[N,N-diphenyl-
There total 3 articles about Benzenamine,
4,4'-[(5-ethenyl-1,3-phenylene)di-2,1-ethenediyl]bis[N,N-diphenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Methyltriphenylphosphonium bromide;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Inert atmosphere;
C47H36N2O;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1246/cl.2012.516
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: palladium diacetate; sodium carbonate; triphenylphosphine / N,N-dimethyl acetamide / 24 h / 110 °C / Inert atmosphere
3.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
3.2: 2 h / 20 °C / Inert atmosphere
With
potassium tert-butylate; palladium diacetate; sodium carbonate; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1246/cl.2012.516
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium diacetate; sodium carbonate; triphenylphosphine / N,N-dimethyl acetamide / 24 h / 110 °C / Inert atmosphere
2.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
2.2: 2 h / 20 °C / Inert atmosphere
With
potassium tert-butylate; palladium diacetate; sodium carbonate; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1246/cl.2012.516
