3-Chloro-3-methyl-1-butyne

Base Information

Chemical Name:3-Chloro-3-methyl-1-butyne
CAS No.:1111-97-3
Molecular Formula:C5H7Cl
Molecular Weight:102.564
Hs Code.:29032990
European Community (EC) Number:214-188-9
NSC Number:16173
DSSTox Substance ID:DTXSID2061488
Nikkaji Number:J217.230E
Wikidata:Q72453843
Mol file:1111-97-3.mol

Synonyms:3-Chloro-3-methyl-1-butyne;1111-97-3;3-Chloro-3-methylbut-1-yne;1-Butyne, 3-chloro-3-methyl-;3-methyl-3-chlorobutyne;2-chloro-2-methyl-3-butyne;2-methyl-2-chloro-3-butyne;3-Chloro-3-methyl-but-1-yne;EINECS 214-188-9;MFCD00190221;NSC 16173;AI3-25133;NSC16173;3-Chloro-3-methyl-1-butyne, 97%;3-Chlor-3-methylbutin;3-chloro-3-methylbutyne;2-chloro-2-methyl butyne;3-chloro-3-methyl butyne;3-chloro-3-methyl-butyne;3-chloro-3-methyl-1-butyn;3-chloro-3,3-dimethylpropyn;3-methyl-3-chlorobut-1-yne;a,a-Dimethylpropargyl chloride;SCHEMBL284084;1,1-Dimethylpropargyl chloride;3-chloro-3-methyl -1-butyne;3-chloro-3-methyl-1 -butyne;3-chloro-3-methyl-but-1-ine;DTXSID2061488;3,3-chloro-3-methylbut-1-yne;2-Methyl-3-butyn-2-yl chloride;AMY19182;BBL102778;NSC-16173;STL556584;AKOS000278712;CS-W013692;FS-4551;FT-0694615;EN300-96068;J-512208;J-650120

Suppliers and Price of 3-Chloro-3-methyl-1-butyne

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Chloro-3-methyl-1-butyne
100g
$ 375.00

Sigma-Aldrich
3-Chloro-3-methyl-1-butyne 97%
5g
$ 120.00

Sigma-Aldrich
3-Chloro-3-methyl-1-butyne 97%
25g
$ 396.00

Medical Isotopes, Inc.
3-Chloro-3-methyl-1-butyne
100 g
$ 875.00

GFS CHEMICALS
3-CHLORO-3-METHYL-1BUTYNE
10 G
$ 210.50

Frontier Specialty Chemicals
3-Chloro-3-methyl-1-butyne 96%
5g
$ 142.00

Frontier Specialty Chemicals
3-Chloro-3-methyl-1-butyne 96%
1g
$ 39.00

Frontier Specialty Chemicals
3-Chloro-3-methyl-1-butyne 96%
25g
$ 477.00

American Custom Chemicals Corporation
3-CHLORO-3-METHYL-1-BUTYNE 95.00%
50G
$ 2783.27

American Custom Chemicals Corporation
3-CHLORO-3-METHYL-1-BUTYNE 95.00%
10G
$ 1194.56

Total 70 raw suppliers

Chemical Property of 3-Chloro-3-methyl-1-butyne

Chemical Property:

Appearance/Colour:Clear colorless to straw colored liquid
Vapor Pressure:104mmHg at 25°C
Melting Point:-61 °C(lit.)
Refractive Index:1.437
Boiling Point:77.999 °C at 760 mmHg
Flash Point:4.444 °C
PSA：0.00000
Density:0.965 g/cm³
LogP:1.63700
Storage Temp.:Refrigerator (+4°C)
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:102.0236279
Heavy Atom Count:6
Complexity:83.4

Purity/Quality:

99% ^*data from raw suppliers

3-Chloro-3-methyl-1-butyne ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn,F,Xi
Hazard Codes:F,Xn,Xi
Statements: 11-20/21/22
Safety Statements: 16-26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CC(C)(C#C)Cl
Uses 3-Chloro-3-methyl-1-butyne is a propargyl chloride used to alkylate methanol, ethanol, ammonia and amines to the corresponding propargylic ether and amines. 3-Chloro-3-methyl-1-butyne was used in preparation of:series of benzo[b]pyrano[2,3-i]xanthen-6-ones and benzo[b]pyrano[3,2-h]xanthen-7-ones6-hydroxy-3,3-dimethyl-3H,7H-benzo[a]pyrano[3,2-h]xanthen-7-one5-hydroxy-2,2-dimethyl-2H,6H-benzo[a]pyrano[2,3-i]xanthen-6-one3,3-dimethyl-3Hbenzofuro[3,2-f][1]-benzopyran

Technology Process of 3-Chloro-3-methyl-1-butyne

There total 12 articles about 3-Chloro-3-methyl-1-butyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.77%

: 115-19-5
2-methyl-but-3-yn-2-ol

: 1111-97-3
3-chloro-3-methylbut-1-yne

Guidance literature:: With hydrogenchloride; iron(III) chloride; isophthalic acid; Benzotrichlorid; copper(l) chloride; In water; at 75 - 85 ℃; for 6h; Temperature; Concentration;

Reference yield: 52.0%

: 1111-97-3
3-chloro-3-methylbut-1-yne

Guidance literature:

Reference yield:

: 598-23-2
3-methyl-but-1-yne

: 1111-97-3
3-chloro-3-methylbut-1-yne

: 624-96-4
1,3-dichloro-3-methylbutane

: 17773-66-9
2,2-Dichlor-3-methylbutan

: 17773-64-7
2-chloro-3-methylbut-1-ene

Guidance literature:: With hydrogenchloride; for 264h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;