13-(4-Nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

Base Information

Chemical Name:13-(4-Nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane
CAS No.:66750-07-0
Molecular Formula:C16H24N2O5
Molecular Weight:324.377
Hs Code.:
DSSTox Substance ID:DTXSID20498763
Wikidata:Q82349028

Synonyms:66750-07-0;DTXSID20498763;13-(4-Nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

Suppliers and Price of 13-(4-Nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 13-(4-Nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

Chemical Property:

XLogP3:0.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:1
Exact Mass:324.16852187
Heavy Atom Count:23
Complexity:295

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCOCCOCCOCCN1C2=CC=C(C=C2)N=O

Technology Process of 13-(4-Nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

There total 2 articles about 13-(4-Nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 66750-10-5
13-phenyl-1,4,7,10-tetraoxa-13-aza-cyclopentadecane

: 66750-07-0
13-(4-nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; for 20h; temp. below 5 deg C;

Reference yield:

: 120-07-0
2,2'-(phenylimino)bis[ethanol]

: 66750-07-0
13-(4-nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 16 percent / NaOH / dioxane / 30 h / Heating

2: 83 percent / 37percent HCl, NaNO₂ / H₂O / 20 h / temp. below 5 deg C

With hydrogenchloride; sodium hydroxide; sodium nitrite; In 1,4-dioxane; water;