Benzenamine, 4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)-

Base Information

• Chemical Name: Benzenamine, 4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)-
• CAS No.: 66750-05-8
• Molecular Formula: C16H26N2O4
• Molecular Weight: 310.393
• DSSTox Substance ID: DTXSID00460322
• Nikkaji Number: J1.730.281G
• Wikidata: Q82284332
• Mol file: 66750-05-8.mol

Synonyms:Benzenamine, 4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)-;66750-05-8;DTXSID00460322

Chemical Property of Benzenamine, 4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)-

Chemical Property:

• XLogP3: 0.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 1
• Exact Mass: 310.18925731
• Heavy Atom Count: 22
• Complexity: 257

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1COCCOCCOCCOCCN1C2=CC=C(C=C2)N

Technology Process of Benzenamine, 4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)-

There total 13 articles about Benzenamine, 4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

13-(4-nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane (66750-07-0) → N-(4-aminophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane (66750-05-8)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; In water; at 40 ℃; for 0.333333h;

Reference yield: 86.0%

N-(4-acetamidophenyl)monoaza-15-crown-5 → N-(4-aminophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane (66750-05-8)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; Heating;

DOI:10.1080/00304940309355838

Reference yield: 85.0%

13-(4-nitrophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane (245125-18-2) → N-(4-aminophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane (66750-05-8)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; In ethyl acetate;

DOI:10.1080/00304940309355838

upstream raw materials:

13-(4-nitrosophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

13-(4-nitrophenyl)-1,4,7,10-tetraoxa-13-azacyclopentadecane

N,N-bis(2-hydroxyethyl)-4-nitroaniline

triethylene glycol di-(p-toluenesulfonate)

Downstream raw materials:

4-<4-(4,7,10,13-Tetraoxa-1-azacyclopentadecyl)phenylimino>-1(4H)-naphthalinon

1,7-Bis<4-(4,7,10,13-tetraoxa-1-azacyclopentadecyl)phenyl>-1,7-diaza-1,3,5-heptatrienyliumchlorid

2-<4-(4,7,10,13-Tetraoxa-1-azacyclopentadecyl)phenylamino>-1,4-naphthochinon

4-<4-(4,7,10,13-Tetraoxa-1-azacyclopentadecyl)phenylimino>-2,5-cyclohexadien-1-on